Zachodniopomorski Uniwersytet Technologiczny w Szczecinie

Szkoła Doktorska - ZUT Doctoral School
specjalność: CHEMICAL ENGINEERING BLOCK

Sylabus przedmiotu Modern methods of chemical analysis:

Informacje podstawowe

Kierunek studiów ZUT Doctoral School
Forma studiów studia stacjonarne Poziom
Stopnień naukowy absolwenta doktor
Obszary studiów charakterystyki PRK
Profil
Moduł —
Przedmiot Modern methods of chemical analysis
Specjalność CHEMICAL ENGINEERING BLOCK
Jednostka prowadząca Katedra Chemii Nieorganicznej i Analitycznej
Nauczyciel odpowiedzialny Elżbieta Filipek <Elzbieta.Filipek@zut.edu.pl>
Inni nauczyciele
ECTS (planowane) 0,5 ECTS (formy) 0,5
Forma zaliczenia zaliczenie Język angielski
Blok obieralny 5 Grupa obieralna 2

Formy dydaktyczne

Forma dydaktycznaKODSemestrGodzinyECTSWagaZaliczenie
wykładyW2 8 0,51,00zaliczenie

Wymagania wstępne

KODWymaganie wstępne
W-1Knowledge in the field of inorganic and organic chemistry and physics at the level of S1 studies

Cele przedmiotu

KODCel modułu/przedmiotu
C-1Presentation of instrumental methods used in studies of the properties of various types of materials
C-2Developing the ability to select an instrumental method to determine properties of the characterized material

Treści programowe z podziałem na formy zajęć

KODTreść programowaGodziny
wykłady
T-W-1X-ray diffraction (XRD) method, applications and interpretation of X-ray diffractograms of selected solids and mixtures.2
T-W-2Thermal analysis methods (DTA, TG, DSC), applications and interpretation of effects on DTA, DSC and TG curves.2
T-W-3Nuclear magnetic resonance (NMR) method and CP MAS spectroscopy in solution and in solid. Applications and interpretation of research results using these methods.2
T-W-4Infrared (IR) spectroscopy method, applications and interpretation of IR spectra.2
8

Obciążenie pracą studenta - formy aktywności

KODForma aktywnościGodziny
wykłady
A-W-1Attending lectures.8
A-W-2Studying the recommended literature concerning the methods discussed during lectures.8
16

Metody nauczania / narzędzia dydaktyczne

KODMetoda nauczania / narzędzie dydaktyczne
M-1Informative lecture
M-2Problem-based lecture

Sposoby oceny

KODSposób oceny
S-1Ocena formująca: attending lectures
S-2Ocena podsumowująca: Written development of a solution to a specific problem (case study).

Zamierzone efekty uczenia się - wiedza

Zamierzone efekty uczenia sięOdniesienie do efektów kształcenia dla dyscyplinyOdniesienie do efektów zdefiniowanych dla obszaru kształceniaCel przedmiotuTreści programoweMetody nauczaniaSposób oceny
ISDE_4-_ICH03.2_W01
Knows modern methods of chemical analysis, with particular emphasis on instrumental methods		ISDE_4-_W02, ISDE_4-_W03—C-1, C-2T-W-1, T-W-2, T-W-3, T-W-4M-1, M-2S-1, S-2

Zamierzone efekty uczenia się - inne kompetencje społeczne i personalne

Zamierzone efekty uczenia sięOdniesienie do efektów kształcenia dla dyscyplinyOdniesienie do efektów zdefiniowanych dla obszaru kształceniaCel przedmiotuTreści programoweMetody nauczaniaSposób oceny
ISDE_4-_ICH03.2_K01
Understands the necessity to analyze research activity and its contribution to the development of the represented filed and discipline.		ISDE_4-_K01—C-1, C-2T-W-1, T-W-2, T-W-3, T-W-4M-1, M-2S-2

Kryterium oceny - wiedza

Efekt uczenia sięOcenaKryterium oceny
ISDE_4-_ICH03.2_W01
Knows modern methods of chemical analysis, with particular emphasis on instrumental methods		2,0
3,0Written solution of an analytical problem
3,5
4,0
4,5
5,0

Kryterium oceny - inne kompetencje społeczne i personalne

Efekt uczenia sięOcenaKryterium oceny
ISDE_4-_ICH03.2_K01
Understands the necessity to analyze research activity and its contribution to the development of the represented filed and discipline.		2,0
3,0Preparation of presentation.
3,5
4,0
4,5
5,0

Literatura podstawowa

  1. Wendlandt, W. W., Thermal analysis, Wiley, New York, 1986
  2. M. E. Brown, Introduction to Thermal Analysis. Techniques and Applications, Kluwer Academic Publishers, Dordrecht, 2001
  3. Frank H. Chung, Deane K. Smith., Industrial applications of X-ray diffraction, Marcel Dekker, 2000
  4. Eberhart, Jean Pierre, Structural and chemical analysis of materials : X-ray, electron and neutron diffraction X-ray..., Wiley, 1995
  5. Nakamoto, K., Infrared and Raman spectra of inorganic and coordination compounds., Wiley, 2009
  6. Iggo J. A., NMR spectroscopy in inorganic chemistry, Oxford University Press, 2020

Literatura dodatkowa

  1. S. Berger, S. Braun, 200 and more basic NMR experiments, Wiley VCH, Weinheim, 2004
  2. E. Breitmaier, Structure elucidation by NMR in organic chemistry, Wiley, Chichester, 1993

Treści programowe - wykłady

KODTreść programowaGodziny
T-W-1X-ray diffraction (XRD) method, applications and interpretation of X-ray diffractograms of selected solids and mixtures.2
T-W-2Thermal analysis methods (DTA, TG, DSC), applications and interpretation of effects on DTA, DSC and TG curves.2
T-W-3Nuclear magnetic resonance (NMR) method and CP MAS spectroscopy in solution and in solid. Applications and interpretation of research results using these methods.2
T-W-4Infrared (IR) spectroscopy method, applications and interpretation of IR spectra.2
8

Formy aktywności - wykłady

KODForma aktywnościGodziny
A-W-1Attending lectures.8
A-W-2Studying the recommended literature concerning the methods discussed during lectures.8
16
(*) 1 punkt ECTS, odpowiada około 30 godzinom aktywności studenta
PoleKODZnaczenie kodu
Zamierzone efekty uczenia sięISDE_4-_ICH03.2_W01Knows modern methods of chemical analysis, with particular emphasis on instrumental methods
Odniesienie do efektów kształcenia dla dyscyplinyISDE_4-_W02They have extended, theory-based knowledge relating to the represented field and discipline and detailed knowledge at an advanced level in the area of scientific research ,methodology of scientific work, preparation of publications and presentations of research results and the principle of dissemination of the results of scientific work, including open access mode.
ISDE_4-_W03They know and understand fundamental dilemmas of modern civilisation, also in relation to the recent scientific developments in the represented field and discipline.
Cel przedmiotuC-1Presentation of instrumental methods used in studies of the properties of various types of materials
C-2Developing the ability to select an instrumental method to determine properties of the characterized material
Treści programoweT-W-1X-ray diffraction (XRD) method, applications and interpretation of X-ray diffractograms of selected solids and mixtures.
T-W-2Thermal analysis methods (DTA, TG, DSC), applications and interpretation of effects on DTA, DSC and TG curves.
T-W-3Nuclear magnetic resonance (NMR) method and CP MAS spectroscopy in solution and in solid. Applications and interpretation of research results using these methods.
T-W-4Infrared (IR) spectroscopy method, applications and interpretation of IR spectra.
Metody nauczaniaM-1Informative lecture
M-2Problem-based lecture
Sposób ocenyS-1Ocena formująca: attending lectures
S-2Ocena podsumowująca: Written development of a solution to a specific problem (case study).
Kryteria ocenyOcenaKryterium oceny
2,0
3,0Written solution of an analytical problem
3,5
4,0
4,5
5,0
PoleKODZnaczenie kodu
Zamierzone efekty uczenia sięISDE_4-_ICH03.2_K01Understands the necessity to analyze research activity and its contribution to the development of the represented filed and discipline.
Odniesienie do efektów kształcenia dla dyscyplinyISDE_4-_K01They understand the necessity and are prepared to critically analyse the achieved scientific output and the contribution of the results of their own research activity to the development of the represented field and discipline.
Cel przedmiotuC-1Presentation of instrumental methods used in studies of the properties of various types of materials
C-2Developing the ability to select an instrumental method to determine properties of the characterized material
Treści programoweT-W-1X-ray diffraction (XRD) method, applications and interpretation of X-ray diffractograms of selected solids and mixtures.
T-W-2Thermal analysis methods (DTA, TG, DSC), applications and interpretation of effects on DTA, DSC and TG curves.
T-W-3Nuclear magnetic resonance (NMR) method and CP MAS spectroscopy in solution and in solid. Applications and interpretation of research results using these methods.
T-W-4Infrared (IR) spectroscopy method, applications and interpretation of IR spectra.
Metody nauczaniaM-1Informative lecture
M-2Problem-based lecture
Sposób ocenyS-2Ocena podsumowująca: Written development of a solution to a specific problem (case study).
Kryteria ocenyOcenaKryterium oceny
2,0
3,0Preparation of presentation.
3,5
4,0
4,5
5,0