ZUT - Krajowe Ramy Kwalifikacji / Rok 2018/2019 / Administracja Centralna Uczelni / Wymiana międzynarodowa (S3) / Sylabus przedmiotu - INSTRUMETAL ANALYSIS IN TOXICOLOGICAL STUDIES

Zachodniopomorski Uniwersytet Technologiczny w Szczecinie

Administracja Centralna Uczelni - Wymiana międzynarodowa (S3)

Sylabus przedmiotu INSTRUMETAL ANALYSIS IN TOXICOLOGICAL STUDIES:

Informacje podstawowe

Kierunek studiów	Wymiana międzynarodowa
Forma studiów	studia stacjonarne	Poziom	trzeciego stopnia
Stopnień naukowy absolwenta
Obszary studiów	studia trzeciego stopnia
Profil
Moduł	—
Przedmiot	INSTRUMETAL ANALYSIS IN TOXICOLOGICAL STUDIES
Specjalność	przedmiot wspólny
Jednostka prowadząca	Katedra Toksykologii, Technologii Mleczarskiej i Przechowalnictwa Żywności
Nauczyciel odpowiedzialny	Artur Ciemniak <Artur.Ciemniak@zut.edu.pl>
Inni nauczyciele	Monika Rajkowska-Myśliwiec <Monika.Rajkowska@zut.edu.pl>
ECTS (planowane)	6,0	ECTS (formy)	6,0
Forma zaliczenia	zaliczenie	Język	angielski
Blok obieralny	—	Grupa obieralna	—

Formy dydaktyczne

Forma dydaktyczna	KOD	Semestr	Godziny	ECTS	Waga	Zaliczenie
laboratoria	L	1	45	6,0	1,00	zaliczenie

Wymagania wstępne

KOD	Wymaganie wstępne
W-1	Knowlege of chemistry, biochemistry, analytical chemistry
W-2	Knowlege of chemistry, biochemistry, analytical chemistry.

Cele przedmiotu

KOD	Cel modułu/przedmiotu
C-1	The student should know the theoretical and practical knowledge of analytical methods (analytical equipment, prepare sample, instrumental analysis and elaboration and discussion of results)

Treści programowe z podziałem na formy zajęć

KOD	Treść programowa	Godziny
laboratoria
T-L-1	Introduction (health and safety, organization of exercises, requirements); Basic equipment and chemicals used in the laboratory. Preparation of solutions of a given concentration. Development and interpretation of measurement results. Quality issues in the analysis.	4
T-L-2	Electrochemical methods in the laboratory	6
T-L-3	Basics knowlege about spectrophotometry. UV-VIS spectra. Collecting spectra, comparing the spectra for solutions of selected substances, the choice of analytical wavelengths. Application in practice.	6
T-L-4	Emission and absorption spectrometry. Heavy metals analysis in food and environment. Preparation of samples, and equipment. Preparation of the calibration curve. Quantitative analysis.	12
T-L-5	Basic chromatographic methods. Sample preparation and analysis. Application in practice. The identification of unknown compounds.	10
T-L-6	Presentation of projects (papers) on the analysis of toxic substances. (Discussion of the planned research methodology, selection of equipment, suppliers, chemicals, laboratory glassware, initial cost calculation).	4
T-L-7	Construction and basic maintenance operations of analytical instruments. Examination	3
		45

Obciążenie pracą studenta - formy aktywności

KOD	Forma aktywności	Godziny
laboratoria
A-L-1	Attendance	45
A-L-2	Preparing for the classes	30
A-L-3	Consultation with the tutor	25
A-L-4	Prepare the reports and project	30
A-L-5	Studying the literature on the subject	30
A-L-6	Prepare to examination	20
		180

Metody nauczania / narzędzia dydaktyczne

KOD	Metoda nauczania / narzędzie dydaktyczne
M-1	Practical exercises

Sposoby oceny

KOD	Sposób oceny
S-1	Ocena formująca: Continuous assessment
S-2	Ocena formująca: Assessment of the students projects.

Zamierzone efekty kształcenia - wiedza

Zamierzone efekty kształcenia	Odniesienie do efektów kształcenia dla dyscypliny	Odniesienie do efektów zdefiniowanych dla obszaru kształcenia	Cel przedmiotu	Treści programowe	Metody nauczania	Sposób oceny
WM_3-_null_W01 Student will gain knowledge of selected methods of instrumental analysis (particularly elektrochemical , spectrophotometric, emission and absorption methods and chromathographic methods)	—	—	C-1	T-L-5, T-L-3, T-L-6, T-L-4, T-L-2	M-1	S-1, S-2

Zamierzone efekty kształcenia - umiejętności

Zamierzone efekty kształcenia	Odniesienie do efektów kształcenia dla dyscypliny	Odniesienie do efektów zdefiniowanych dla obszaru kształcenia	Cel przedmiotu	Treści programowe	Metody nauczania	Sposób oceny
WM_3-_null_U01 Student is able to use the catalogs of equipment, instruments and reagents. He is able to design and conduct an analysis using instrumental techniques involving supervised. Student can, independently elaborate the results and formulate conclusions.	—	—	C-1	T-L-5, T-L-7, T-L-3, T-L-6, T-L-4, T-L-2	M-1	S-1, S-2

Zamierzone efekty kształcenia - inne kompetencje społeczne i personalne

Zamierzone efekty kształcenia	Odniesienie do efektów kształcenia dla dyscypliny	Odniesienie do efektów zdefiniowanych dla obszaru kształcenia	Cel przedmiotu	Treści programowe	Metody nauczania	Sposób oceny
WM_3-_null_K01 He cares about the effects of their work. It is aware of the professional and ethical responsibility for the results of their analysis.	—	—	C-1	T-L-1	M-1	S-1, S-2

Kryterium oceny - wiedza

Efekt kształcenia	Ocena	Kryterium oceny
WM_3-_null_W01 Student will gain knowledge of selected methods of instrumental analysis (particularly elektrochemical , spectrophotometric, emission and absorption methods and chromathographic methods)	2,0
	3,0	The student has to define and describe presented methods and problems
	3,5
	4,0
	4,5
	5,0

Kryterium oceny - umiejętności

Efekt kształcenia	Ocena	Kryterium oceny
WM_3-_null_U01 Student is able to use the catalogs of equipment, instruments and reagents. He is able to design and conduct an analysis using instrumental techniques involving supervised. Student can, independently elaborate the results and formulate conclusions.	2,0
	3,0	The student is able to use the presented methods
	3,5
	4,0
	4,5
	5,0

Literatura podstawowa

Holler, F. James; Skoog Douglas A; West Donald M., Fundamentals of analytical chemistry., Saunders College Pub, Philadelphia, 1996, ISBN 0-03-005938-0
Nieman Timothy A.; Skoog, Douglas A.;p Holler F. James, principles of instrumental analysis., Pacific Grove, CA: Brooks/Cole, 1996, ISBN 0-03-002078-6
Journals (for example: Analytical Ciemistry, Talanta, etc.

Treści programowe - laboratoria

KOD	Treść programowa	Godziny
T-L-1	Introduction (health and safety, organization of exercises, requirements); Basic equipment and chemicals used in the laboratory. Preparation of solutions of a given concentration. Development and interpretation of measurement results. Quality issues in the analysis.	4
T-L-2	Electrochemical methods in the laboratory	6
T-L-3	Basics knowlege about spectrophotometry. UV-VIS spectra. Collecting spectra, comparing the spectra for solutions of selected substances, the choice of analytical wavelengths. Application in practice.	6
T-L-4	Emission and absorption spectrometry. Heavy metals analysis in food and environment. Preparation of samples, and equipment. Preparation of the calibration curve. Quantitative analysis.	12
T-L-5	Basic chromatographic methods. Sample preparation and analysis. Application in practice. The identification of unknown compounds.	10
T-L-6	Presentation of projects (papers) on the analysis of toxic substances. (Discussion of the planned research methodology, selection of equipment, suppliers, chemicals, laboratory glassware, initial cost calculation).	4
T-L-7	Construction and basic maintenance operations of analytical instruments. Examination	3
		45

Formy aktywności - laboratoria

KOD	Forma aktywności	Godziny
A-L-1	Attendance	45
A-L-2	Preparing for the classes	30
A-L-3	Consultation with the tutor	25
A-L-4	Prepare the reports and project	30
A-L-5	Studying the literature on the subject	30
A-L-6	Prepare to examination	20
		180

(*) 1 punkt ECTS, odpowiada około 30 godzinom aktywności studenta

Pole	KOD	Znaczenie kodu
Zamierzone efekty kształcenia	WM_3-_null_W01	Student will gain knowledge of selected methods of instrumental analysis (particularly elektrochemical , spectrophotometric, emission and absorption methods and chromathographic methods)
Cel przedmiotu	C-1	The student should know the theoretical and practical knowledge of analytical methods (analytical equipment, prepare sample, instrumental analysis and elaboration and discussion of results)
Treści programowe	T-L-5	Basic chromatographic methods. Sample preparation and analysis. Application in practice. The identification of unknown compounds.
	T-L-3	Basics knowlege about spectrophotometry. UV-VIS spectra. Collecting spectra, comparing the spectra for solutions of selected substances, the choice of analytical wavelengths. Application in practice.
	T-L-6	Presentation of projects (papers) on the analysis of toxic substances. (Discussion of the planned research methodology, selection of equipment, suppliers, chemicals, laboratory glassware, initial cost calculation).
	T-L-4	Emission and absorption spectrometry. Heavy metals analysis in food and environment. Preparation of samples, and equipment. Preparation of the calibration curve. Quantitative analysis.
	T-L-2	Electrochemical methods in the laboratory
Metody nauczania	M-1	Practical exercises
Sposób oceny	S-1	Ocena formująca: Continuous assessment
Sposób oceny	S-2	Ocena formująca: Assessment of the students projects.
Kryteria oceny	Ocena	Kryterium oceny
	2,0
	3,0	The student has to define and describe presented methods and problems
	3,5
	4,0
	4,5
	5,0

Pole	KOD	Znaczenie kodu
Zamierzone efekty kształcenia	WM_3-_null_U01	Student is able to use the catalogs of equipment, instruments and reagents. He is able to design and conduct an analysis using instrumental techniques involving supervised. Student can, independently elaborate the results and formulate conclusions.
Cel przedmiotu	C-1	The student should know the theoretical and practical knowledge of analytical methods (analytical equipment, prepare sample, instrumental analysis and elaboration and discussion of results)
Treści programowe	T-L-5	Basic chromatographic methods. Sample preparation and analysis. Application in practice. The identification of unknown compounds.
	T-L-7	Construction and basic maintenance operations of analytical instruments. Examination
	T-L-3	Basics knowlege about spectrophotometry. UV-VIS spectra. Collecting spectra, comparing the spectra for solutions of selected substances, the choice of analytical wavelengths. Application in practice.
	T-L-6	Presentation of projects (papers) on the analysis of toxic substances. (Discussion of the planned research methodology, selection of equipment, suppliers, chemicals, laboratory glassware, initial cost calculation).
	T-L-4	Emission and absorption spectrometry. Heavy metals analysis in food and environment. Preparation of samples, and equipment. Preparation of the calibration curve. Quantitative analysis.
	T-L-2	Electrochemical methods in the laboratory
Metody nauczania	M-1	Practical exercises
Sposób oceny	S-1	Ocena formująca: Continuous assessment
Sposób oceny	S-2	Ocena formująca: Assessment of the students projects.
Kryteria oceny	Ocena	Kryterium oceny
	2,0
	3,0	The student is able to use the presented methods
	3,5
	4,0
	4,5
	5,0

Pole	KOD	Znaczenie kodu
Zamierzone efekty kształcenia	WM_3-_null_K01	He cares about the effects of their work. It is aware of the professional and ethical responsibility for the results of their analysis.
Cel przedmiotu	C-1	The student should know the theoretical and practical knowledge of analytical methods (analytical equipment, prepare sample, instrumental analysis and elaboration and discussion of results)
Treści programowe	T-L-1	Introduction (health and safety, organization of exercises, requirements); Basic equipment and chemicals used in the laboratory. Preparation of solutions of a given concentration. Development and interpretation of measurement results. Quality issues in the analysis.
Metody nauczania	M-1	Practical exercises
Sposób oceny	S-1	Ocena formująca: Continuous assessment
Sposób oceny	S-2	Ocena formująca: Assessment of the students projects.