Zachodniopomorski Uniwersytet Technologiczny w Szczecinie

Wydział Technologii i Inżynierii Chemicznej - Materials Science and Engineering (S1)

Sylabus przedmiotu Intro to Materials Synthesis and Products Analysis:

Informacje podstawowe

Kierunek studiów Materials Science and Engineering
Forma studiów studia stacjonarne Poziom pierwszego stopnia
Tytuł zawodowy absolwenta inżynier
Obszary studiów charakterystyki PRK, kompetencje inżynierskie PRK
Profil ogólnoakademicki
Moduł —
Przedmiot Intro to Materials Synthesis and Products Analysis
Specjalność przedmiot wspólny
Jednostka prowadząca Katedra Chemii Organicznej i Chemii Fizycznej
Nauczyciel odpowiedzialny Jacek Sośnicki <Jacek.Sosnicki@zut.edu.pl>
Inni nauczyciele
ECTS (planowane) 7,0 ECTS (formy) 7,0
Forma zaliczenia egzamin Język angielski
Blok obieralny — Grupa obieralna —

Formy dydaktyczne

Forma dydaktycznaKODSemestrGodzinyECTSWagaZaliczenie
wykładyW3 30 2,00,25egzamin
ćwiczenia audytoryjneA3 30 2,00,25zaliczenie
laboratoriaL3 30 3,00,50zaliczenie

Wymagania wstępne

KODWymaganie wstępne
W-1Basic knowledge of organic chemistry.

Cele przedmiotu

KODCel modułu/przedmiotu
C-1The student knows how to carry out a basic literature search based on databases and scientific literature.
C-2The student is able to conduct the synthesis of the simple organic compound/material and knows standard methods for their analysis and can prepare the report.
C-3The student is aware of the importance of the knowledge acquired within the subject for developement of science and for improvement of the quality of life.

Treści programowe z podziałem na formy zajęć

KODTreść programowaGodziny
ćwiczenia audytoryjne
T-A-1Exercises in planning synthesis of the simple and complex organic molecules through functional group transformations with the use of databases.15
T-A-2Exercises in determining the structure of organic compounds by IR, NMR, MS methods.15
30
laboratoria
T-L-1Regulations and safety rules in the laboratory of organic synthesis.2
T-L-2Practical aspects of purification and structural analysis (by IR, MS, NMR) of organic compounds. (Sample preparation, selection of purification method and measurement conditions, etc.)5
T-L-3Building a carbon skeleton by using organometallic compounds. Eg. Application of Sonogashira reaction in the preparation of alkyne. Purification of the product with a properly selected method. Structure analysis by spectroscopic methods (IR, MS, NMR).18
T-L-4Elemental analysis, determination of C, N and S in organic materials, microwave mineralization and determination of elemental composition by ICP-OES method.5
30
wykłady
T-W-1Databases and scientific journals as a platform to start organic material synthesis.1
T-W-2Principles of planning the synthesis of simple and complex organic molecules.1
T-W-3Functional group transformations – an introduction to the synthesis of complex organic compounds and organic materials (e.g. based on coupling, condensation, addition, substitution and elimination reactions)6
T-W-4The synthesis of functionalized arenes, heteroarenes as well as other carbo- and heterocyclic compounds.4
T-W-5The synthesis of functionalized monomers based on organometallic chemistry.3
T-W-6Isolation and separation techniques of organic compounds and organic materials.2
T-W-7Overview of IR, MS and NMR as fundamental methods for analysis of organic compounds.8
T-W-8Analysis of the elemental composition of organic materials (elemental analyzers C, N, S, ICP and XRF methods)5
30

Obciążenie pracą studenta - formy aktywności

KODForma aktywnościGodziny
ćwiczenia audytoryjne
A-A-1Participation in recitations30
A-A-2Self-improvement by solving additional problems.26
A-A-3Face to face discussion.4
60
laboratoria
A-L-1Participation in the laboratory classes.30
A-L-2Self-study of recomended literature.26
A-L-3Face to face discussion.4
A-L-4Theoretical preparation to the laboratory classes.20
A-L-5Preparation of written reports.10
90
wykłady
A-W-1Participation in the lectures.30
A-W-2Self study of recomended literature.26
A-W-3Consultations.4
A-W-4The exam1
61

Metody nauczania / narzędzia dydaktyczne

KODMetoda nauczania / narzędzie dydaktyczne
M-1Lecture with discussion.
M-2Classes with discussion.
M-3Laboratory exercises.

Sposoby oceny

KODSposób oceny
S-1Ocena formująca: Continuous assessment: laboratory reports and activity.
S-2Ocena podsumowująca: Exam.
S-3Ocena podsumowująca: Final test.

Zamierzone efekty uczenia się - wiedza

Zamierzone efekty uczenia sięOdniesienie do efektów kształcenia dla kierunku studiówOdniesienie do efektów zdefiniowanych dla obszaru kształceniaOdniesienie do efektów uczenia się prowadzących do uzyskania tytułu zawodowego inżynieraCel przedmiotuTreści programoweMetody nauczaniaSposób oceny
MSE_1A_C03_W01
The studen has basic knowledge on the structure, reactivity of simple organic compounds, knows basic methods for purification and instrumental methods for analyses of organic compounds.		MSE_1A_W02, MSE_1A_W03, MSE_1A_W05, MSE_1A_W06——C-2, C-3T-W-7, T-W-3, T-W-4, T-W-5, T-W-6, T-W-8, T-L-4, T-L-3, T-L-2, T-A-2M-1, M-2, M-3S-1, S-2, S-3

Zamierzone efekty uczenia się - umiejętności

Zamierzone efekty uczenia sięOdniesienie do efektów kształcenia dla kierunku studiówOdniesienie do efektów zdefiniowanych dla obszaru kształceniaOdniesienie do efektów uczenia się prowadzących do uzyskania tytułu zawodowego inżynieraCel przedmiotuTreści programoweMetody nauczaniaSposób oceny
MSE_1A_C03_U01
The studen is able to plan and perform basic synthetic transformations on the basis of informations taken from databases and scientific literature.		MSE_1A_U01, MSE_1A_U05, MSE_1A_U06, MSE_1A_U09, MSE_1A_U12——C-1, C-3T-W-1, T-W-3, T-W-4, T-W-5, T-W-2, T-L-1, T-L-3, T-L-2, T-A-1M-1, M-2S-3
MSE_1A_C03_U02
The studen is able to prepare the basic laboratory report.		MSE_1A_U03——C-2T-L-4, T-L-1, T-L-3, T-L-2M-3S-1

Zamierzone efekty uczenia się - inne kompetencje społeczne i personalne

Zamierzone efekty uczenia sięOdniesienie do efektów kształcenia dla kierunku studiówOdniesienie do efektów zdefiniowanych dla obszaru kształceniaOdniesienie do efektów uczenia się prowadzących do uzyskania tytułu zawodowego inżynieraCel przedmiotuTreści programoweMetody nauczaniaSposób oceny
MSE_1A_C03_K01
The student is aware of the importance of organic chemistry in life and science.		MSE_1A_K01, MSE_1A_K02——C-3T-W-7, T-W-1, T-W-3, T-W-4, T-W-5, T-W-6, T-W-8, T-L-1M-1, M-2, M-3S-2, S-3

Kryterium oceny - wiedza

Efekt uczenia sięOcenaKryterium oceny
MSE_1A_C03_W01
The studen has basic knowledge on the structure, reactivity of simple organic compounds, knows basic methods for purification and instrumental methods for analyses of organic compounds.		2,0
3,0Positive grade of the final test and exam (more than 55% correct answers)
3,5
4,0
4,5
5,0

Kryterium oceny - umiejętności

Efekt uczenia sięOcenaKryterium oceny
MSE_1A_C03_U01
The studen is able to plan and perform basic synthetic transformations on the basis of informations taken from databases and scientific literature.		2,0
3,0Positive grade of the final test (more than 55% correct answers)
3,5
4,0
4,5
5,0
MSE_1A_C03_U02
The studen is able to prepare the basic laboratory report.		2,0
3,0Positive evaluation of the laboratoty report..
3,5
4,0
4,5
5,0

Kryterium oceny - inne kompetencje społeczne i personalne

Efekt uczenia sięOcenaKryterium oceny
MSE_1A_C03_K01
The student is aware of the importance of organic chemistry in life and science.		2,0
3,0Positive grade of the final test and exam (more than 55% correct answers)
3,5
4,0
4,5
5,0

Literatura podstawowa

  1. John McMurry, Organic Chemistry, Brooks/cole, 2012, 8e
  2. J. J. Li, C. Limberakis, D. A. Pflum, Modern Organic Synthesis in the laboratory. A collection of standard experimental procedures, OXFORD University Press, 2007
  3. Clayden, Greeves, Warren, Wothers, Organic Chemistry, Oxford, 2004
  4. K. Peter C. Vollhardt, Organic Chemistry Structure and Function, W. H. Freeman, 2014

Literatura dodatkowa

  1. Jacques Mortier, Arene Chemistry, Wiley, 2016
  2. W. CARRUTHERS, IAIN COLDHAM, MODERN METHODS OF ORGANIC SYNTHESIS, Cambridge University Press, 2004

Treści programowe - ćwiczenia audytoryjne

KODTreść programowaGodziny
T-A-1Exercises in planning synthesis of the simple and complex organic molecules through functional group transformations with the use of databases.15
T-A-2Exercises in determining the structure of organic compounds by IR, NMR, MS methods.15
30

Treści programowe - laboratoria

KODTreść programowaGodziny
T-L-1Regulations and safety rules in the laboratory of organic synthesis.2
T-L-2Practical aspects of purification and structural analysis (by IR, MS, NMR) of organic compounds. (Sample preparation, selection of purification method and measurement conditions, etc.)5
T-L-3Building a carbon skeleton by using organometallic compounds. Eg. Application of Sonogashira reaction in the preparation of alkyne. Purification of the product with a properly selected method. Structure analysis by spectroscopic methods (IR, MS, NMR).18
T-L-4Elemental analysis, determination of C, N and S in organic materials, microwave mineralization and determination of elemental composition by ICP-OES method.5
30

Treści programowe - wykłady

KODTreść programowaGodziny
T-W-1Databases and scientific journals as a platform to start organic material synthesis.1
T-W-2Principles of planning the synthesis of simple and complex organic molecules.1
T-W-3Functional group transformations – an introduction to the synthesis of complex organic compounds and organic materials (e.g. based on coupling, condensation, addition, substitution and elimination reactions)6
T-W-4The synthesis of functionalized arenes, heteroarenes as well as other carbo- and heterocyclic compounds.4
T-W-5The synthesis of functionalized monomers based on organometallic chemistry.3
T-W-6Isolation and separation techniques of organic compounds and organic materials.2
T-W-7Overview of IR, MS and NMR as fundamental methods for analysis of organic compounds.8
T-W-8Analysis of the elemental composition of organic materials (elemental analyzers C, N, S, ICP and XRF methods)5
30

Formy aktywności - ćwiczenia audytoryjne

KODForma aktywnościGodziny
A-A-1Participation in recitations30
A-A-2Self-improvement by solving additional problems.26
A-A-3Face to face discussion.4
60
(*) 1 punkt ECTS, odpowiada około 30 godzinom aktywności studenta

Formy aktywności - laboratoria

KODForma aktywnościGodziny
A-L-1Participation in the laboratory classes.30
A-L-2Self-study of recomended literature.26
A-L-3Face to face discussion.4
A-L-4Theoretical preparation to the laboratory classes.20
A-L-5Preparation of written reports.10
90
(*) 1 punkt ECTS, odpowiada około 30 godzinom aktywności studenta

Formy aktywności - wykłady

KODForma aktywnościGodziny
A-W-1Participation in the lectures.30
A-W-2Self study of recomended literature.26
A-W-3Consultations.4
A-W-4The exam1
61
(*) 1 punkt ECTS, odpowiada około 30 godzinom aktywności studenta
PoleKODZnaczenie kodu
Zamierzone efekty uczenia sięMSE_1A_C03_W01The studen has basic knowledge on the structure, reactivity of simple organic compounds, knows basic methods for purification and instrumental methods for analyses of organic compounds.
Odniesienie do efektów kształcenia dla kierunku studiówMSE_1A_W02knows selected issues from physics, basic biology and chemistry necessary to describe the properties of materials and processes accompanying their production and processing
MSE_1A_W03knows selected issues concerning the structure of materials, thier synthesis, processing and structure-properties relationship
MSE_1A_W05knows the principles of design, modelling, simulation and understands the principles of basic methods, research tools and techniques (including information technology) used to solve simple engineering tasks in materials engineering
MSE_1A_W06knows the methods of structure characterization and properties evaluation of materials
Cel przedmiotuC-2The student is able to conduct the synthesis of the simple organic compound/material and knows standard methods for their analysis and can prepare the report.
C-3The student is aware of the importance of the knowledge acquired within the subject for developement of science and for improvement of the quality of life.
Treści programoweT-W-7Overview of IR, MS and NMR as fundamental methods for analysis of organic compounds.
T-W-3Functional group transformations – an introduction to the synthesis of complex organic compounds and organic materials (e.g. based on coupling, condensation, addition, substitution and elimination reactions)
T-W-4The synthesis of functionalized arenes, heteroarenes as well as other carbo- and heterocyclic compounds.
T-W-5The synthesis of functionalized monomers based on organometallic chemistry.
T-W-6Isolation and separation techniques of organic compounds and organic materials.
T-W-8Analysis of the elemental composition of organic materials (elemental analyzers C, N, S, ICP and XRF methods)
T-L-4Elemental analysis, determination of C, N and S in organic materials, microwave mineralization and determination of elemental composition by ICP-OES method.
T-L-3Building a carbon skeleton by using organometallic compounds. Eg. Application of Sonogashira reaction in the preparation of alkyne. Purification of the product with a properly selected method. Structure analysis by spectroscopic methods (IR, MS, NMR).
T-L-2Practical aspects of purification and structural analysis (by IR, MS, NMR) of organic compounds. (Sample preparation, selection of purification method and measurement conditions, etc.)
T-A-2Exercises in determining the structure of organic compounds by IR, NMR, MS methods.
Metody nauczaniaM-1Lecture with discussion.
M-2Classes with discussion.
M-3Laboratory exercises.
Sposób ocenyS-1Ocena formująca: Continuous assessment: laboratory reports and activity.
S-2Ocena podsumowująca: Exam.
S-3Ocena podsumowująca: Final test.
Kryteria ocenyOcenaKryterium oceny
2,0
3,0Positive grade of the final test and exam (more than 55% correct answers)
3,5
4,0
4,5
5,0
PoleKODZnaczenie kodu
Zamierzone efekty uczenia sięMSE_1A_C03_U01The studen is able to plan and perform basic synthetic transformations on the basis of informations taken from databases and scientific literature.
Odniesienie do efektów kształcenia dla kierunku studiówMSE_1A_U01being able to use the acquired knowledge related to the engineering of materials to formulate and solve comples and unusual engineering tasks with respect to: - proper selection of sources and information, assessment, critical analysis and synthesis of this information, - selection and application of appropriate methods and tools, including advanced information and communication techniques
MSE_1A_U05being able to use specialized computer software for designing, modelling and computer simulation of selected issues typical for the filed of study
MSE_1A_U06being able to perceive systemic and non-technical aspects, including environmental, economic and ethical aspects of implementing specific technical solutions, and knows the principles of accupational health and safety
MSE_1A_U09is able to critically analyze and elavuate existing technical solutions in the field of materials science and engineering
MSE_1A_U12is able to plan and organize work, both individually and as a team, and interact with other people as part of a team (also of an interdisciplinary nature)
Cel przedmiotuC-1The student knows how to carry out a basic literature search based on databases and scientific literature.
C-3The student is aware of the importance of the knowledge acquired within the subject for developement of science and for improvement of the quality of life.
Treści programoweT-W-1Databases and scientific journals as a platform to start organic material synthesis.
T-W-3Functional group transformations – an introduction to the synthesis of complex organic compounds and organic materials (e.g. based on coupling, condensation, addition, substitution and elimination reactions)
T-W-4The synthesis of functionalized arenes, heteroarenes as well as other carbo- and heterocyclic compounds.
T-W-5The synthesis of functionalized monomers based on organometallic chemistry.
T-W-2Principles of planning the synthesis of simple and complex organic molecules.
T-L-1Regulations and safety rules in the laboratory of organic synthesis.
T-L-3Building a carbon skeleton by using organometallic compounds. Eg. Application of Sonogashira reaction in the preparation of alkyne. Purification of the product with a properly selected method. Structure analysis by spectroscopic methods (IR, MS, NMR).
T-L-2Practical aspects of purification and structural analysis (by IR, MS, NMR) of organic compounds. (Sample preparation, selection of purification method and measurement conditions, etc.)
T-A-1Exercises in planning synthesis of the simple and complex organic molecules through functional group transformations with the use of databases.
Metody nauczaniaM-1Lecture with discussion.
M-2Classes with discussion.
Sposób ocenyS-3Ocena podsumowująca: Final test.
Kryteria ocenyOcenaKryterium oceny
2,0
3,0Positive grade of the final test (more than 55% correct answers)
3,5
4,0
4,5
5,0
PoleKODZnaczenie kodu
Zamierzone efekty uczenia sięMSE_1A_C03_U02The studen is able to prepare the basic laboratory report.
Odniesienie do efektów kształcenia dla kierunku studiówMSE_1A_U03being able to use the principles and methods of chemistry, biology, physics and materials engineering in planning and conducting experiments, is able to interpret and elaborate the results and draw conclusions
Cel przedmiotuC-2The student is able to conduct the synthesis of the simple organic compound/material and knows standard methods for their analysis and can prepare the report.
Treści programoweT-L-4Elemental analysis, determination of C, N and S in organic materials, microwave mineralization and determination of elemental composition by ICP-OES method.
T-L-1Regulations and safety rules in the laboratory of organic synthesis.
T-L-3Building a carbon skeleton by using organometallic compounds. Eg. Application of Sonogashira reaction in the preparation of alkyne. Purification of the product with a properly selected method. Structure analysis by spectroscopic methods (IR, MS, NMR).
T-L-2Practical aspects of purification and structural analysis (by IR, MS, NMR) of organic compounds. (Sample preparation, selection of purification method and measurement conditions, etc.)
Metody nauczaniaM-3Laboratory exercises.
Sposób ocenyS-1Ocena formująca: Continuous assessment: laboratory reports and activity.
Kryteria ocenyOcenaKryterium oceny
2,0
3,0Positive evaluation of the laboratoty report..
3,5
4,0
4,5
5,0
PoleKODZnaczenie kodu
Zamierzone efekty uczenia sięMSE_1A_C03_K01The student is aware of the importance of organic chemistry in life and science.
Odniesienie do efektów kształcenia dla kierunku studiówMSE_1A_K01is able to critically assess the knowledge and content received
MSE_1A_K02acknowledges the importance of knowledge in solving cognitive and practical problems and is able to consult with experts if it is difficult to solve the problem on its own
Cel przedmiotuC-3The student is aware of the importance of the knowledge acquired within the subject for developement of science and for improvement of the quality of life.
Treści programoweT-W-7Overview of IR, MS and NMR as fundamental methods for analysis of organic compounds.
T-W-1Databases and scientific journals as a platform to start organic material synthesis.
T-W-3Functional group transformations – an introduction to the synthesis of complex organic compounds and organic materials (e.g. based on coupling, condensation, addition, substitution and elimination reactions)
T-W-4The synthesis of functionalized arenes, heteroarenes as well as other carbo- and heterocyclic compounds.
T-W-5The synthesis of functionalized monomers based on organometallic chemistry.
T-W-6Isolation and separation techniques of organic compounds and organic materials.
T-W-8Analysis of the elemental composition of organic materials (elemental analyzers C, N, S, ICP and XRF methods)
T-L-1Regulations and safety rules in the laboratory of organic synthesis.
Metody nauczaniaM-1Lecture with discussion.
M-2Classes with discussion.
M-3Laboratory exercises.
Sposób ocenyS-2Ocena podsumowująca: Exam.
S-3Ocena podsumowująca: Final test.
Kryteria ocenyOcenaKryterium oceny
2,0
3,0Positive grade of the final test and exam (more than 55% correct answers)
3,5
4,0
4,5
5,0