Zachodniopomorski Uniwersytet Technologiczny w Szczecinie

Wydział Technologii i Inżynierii Chemicznej - Chemical Engineering (S1)

Sylabus przedmiotu Introduction to Experimental Chemical Technology:

Informacje podstawowe

Kierunek studiów Chemical Engineering
Forma studiów studia stacjonarne Poziom pierwszego stopnia
Tytuł zawodowy absolwenta inżynier
Obszary studiów charakterystyki PRK, kompetencje inżynierskie PRK
Profil ogólnoakademicki
Moduł
Przedmiot Introduction to Experimental Chemical Technology
Specjalność przedmiot wspólny
Jednostka prowadząca Katedra Technologii Chemicznej Nieorganicznej i Inżynierii Środowiska
Nauczyciel odpowiedzialny Rafał Wróbel <Rafal.Wrobel@zut.edu.pl>
Inni nauczyciele Marcin Bartkowiak <Marcin.Bartkowiak@zut.edu.pl>, Dariusz Moszyński <Dariusz.Moszynski@zut.edu.pl>, Rafał Wróbel <Rafal.Wrobel@zut.edu.pl>
ECTS (planowane) 4,0 ECTS (formy) 4,0
Forma zaliczenia zaliczenie Język angielski
Blok obieralny 6 Grupa obieralna 2

Formy dydaktyczne

Forma dydaktycznaKODSemestrGodzinyECTSWagaZaliczenie
laboratoriaL4 45 3,00,50zaliczenie
wykładyW4 15 1,00,50zaliczenie

Wymagania wstępne

KODWymaganie wstępne
W-1basics of chemistry
W-2Advanced mathematics
W-3basics of physics

Cele przedmiotu

KODCel modułu/przedmiotu
C-1Getting knowledge about analytical methods applied in Chemical Technology

Treści programowe z podziałem na formy zajęć

KODTreść programowaGodziny
laboratoria
T-L-1Reaction exhaust gases – MS analysis5
T-L-2Reactivation of catalyst for ammonia synthesis5
T-L-3Activation of heterogeneous catalyst based on cobalt compounds5
T-L-4XRD phase analysis catalysts5
T-L-5SEM analysis of catalysts5
T-L-6XRF analysis of catalysts5
T-L-7Deep oxidation methods in waste water treatment5
T-L-8GC and GC-MS methods as a methods for separation and analysis5
T-L-9FTIR analysis of the products5
45
wykłady
T-W-1Instrumental methods of chemical composition analysis. Selecting of a proper analytical methods. Theoretical basics of atomic spectroscopy. Inductively Coupled Plasma, ICP. Atomic absorption spectroscopy, AAS. Molecular spectra method. Infrared Spectroscopy, FTIR, UV-VIS Spectroscopy, Raman Spectroscopy RS. X-ray methods. X-Ray Fluorescence, XRF, X-Ray Microanalysis; GC and GC-MS in separation and analysis of post-reaction mixtures.4
T-W-2Chemical analysis of the surface of solid state. Physicochemical basics of Electro-spectroscopy methods. Methods: Electron Spectroscopy for Chemical Analysis, ESCA, including X-ray Photoelectron Spectroscopy, XPS, and Ultraviolet Photoemission Spectroscopy, UPS; Auger Electron Spectroscopy, AES, Electron Energy Loss Spectroscopy.4
T-W-3Adsorption/desorption methods and temperature programmed techniques. Thermogravimetry, TG, Temperature Programmed Desorption, TPD, Temperature Programmed Oxidation, TPO, Temperature Programmed Reduction, TPR, Temperature Programmed Surface Reaction, TPSR. Mass spectrometry.3
T-W-4Analysis of phase composition, structure and topography. X-Ray Diffraction, XRD, Reflection High Energy Electron Diffraction, RHEED, Low Energy Electron Diffraction, LEED. Mössbauer Spectroscopy. Scanning Electron Microscopy, SEM, and Transmission Electron Microscopy, TEM, Atomic Force Microscopy, AFM.4
15

Obciążenie pracą studenta - formy aktywności

KODForma aktywnościGodziny
laboratoria
A-L-1Participation in laboratory classes45
A-L-2Data evaluation and preparation of raports28
A-L-3Consultations2
75
wykłady
A-W-1Obligatory attendance the lactures15
A-W-2Repetition of the material8
A-W-3Consultations2
25

Metody nauczania / narzędzia dydaktyczne

KODMetoda nauczania / narzędzie dydaktyczne
M-1Lecture
M-2Laboratory classes

Sposoby oceny

KODSposób oceny
S-1Ocena podsumowująca: Written exam
S-2Ocena formująca: approbation
S-3Ocena podsumowująca: raport

Zamierzone efekty uczenia się - wiedza

Zamierzone efekty uczenia sięOdniesienie do efektów kształcenia dla kierunku studiówOdniesienie do efektów zdefiniowanych dla obszaru kształceniaOdniesienie do efektów uczenia się prowadzących do uzyskania tytułu zawodowego inżynieraCel przedmiotuTreści programoweMetody nauczaniaSposób oceny
ChEn_1A_C09b_W01
Student knows theory required to design basic chemical technology process in laboratory scale.
ChEn_1A_W07, ChEn_1A_W11, ChEn_1A_W08, ChEn_1A_W06C-1T-W-1, T-W-2, T-W-4, T-W-3M-1S-1

Zamierzone efekty uczenia się - umiejętności

Zamierzone efekty uczenia sięOdniesienie do efektów kształcenia dla kierunku studiówOdniesienie do efektów zdefiniowanych dla obszaru kształceniaOdniesienie do efektów uczenia się prowadzących do uzyskania tytułu zawodowego inżynieraCel przedmiotuTreści programoweMetody nauczaniaSposób oceny
ChEn_1A_C09b_U01
Student is able to mount basic laboratory scale instalation used in chemical technology and evaluate the obtained data with mother IT tools.
ChEn_1A_U01, ChEn_1A_U03, ChEn_1A_U05, ChEn_1A_U08, ChEn_1A_U09, ChEn_1A_U16C-1T-L-1, T-L-2, T-L-3, T-L-4, T-L-5, T-L-6, T-L-7, T-L-8, T-L-9M-1S-2

Zamierzone efekty uczenia się - inne kompetencje społeczne i personalne

Zamierzone efekty uczenia sięOdniesienie do efektów kształcenia dla kierunku studiówOdniesienie do efektów zdefiniowanych dla obszaru kształceniaOdniesienie do efektów uczenia się prowadzących do uzyskania tytułu zawodowego inżynieraCel przedmiotuTreści programoweMetody nauczaniaSposób oceny
ChEn_1A_C09b_K01
Student is able to work in team in designing the chemical technology laboratory scale setups.
ChEn_1A_K01, ChEn_1A_K03, ChEn_1A_K04, ChEn_1A_K05C-1T-W-1, T-W-2, T-W-4, T-W-3M-1S-2

Kryterium oceny - wiedza

Efekt uczenia sięOcenaKryterium oceny
ChEn_1A_C09b_W01
Student knows theory required to design basic chemical technology process in laboratory scale.
2,0
3,0Student deliver at least 60% of correct answers
3,5
4,0
4,5
5,0

Kryterium oceny - umiejętności

Efekt uczenia sięOcenaKryterium oceny
ChEn_1A_C09b_U01
Student is able to mount basic laboratory scale instalation used in chemical technology and evaluate the obtained data with mother IT tools.
2,0
3,0Student is able to choose analytical method to solve specific problem
3,5
4,0
4,5
5,0

Kryterium oceny - inne kompetencje społeczne i personalne

Efekt uczenia sięOcenaKryterium oceny
ChEn_1A_C09b_K01
Student is able to work in team in designing the chemical technology laboratory scale setups.
2,0
3,0Student is able to cooperate in team durign problem solving
3,5
4,0
4,5
5,0

Literatura podstawowa

  1. John A. Dean, Analytical Chemistry Handbook, McGraw-Hill Companies, 2000
  2. Peter R. Griffiths, James A. de Haseth., Fourier transform infrared spectrometry, John Wiley & Sons, Hoboken, 2007, 2nd
  3. Helmut Günzler, Alex Williams, Handbook of Analytical Techniques, Wiley-VCH, 2001
  4. Paul N. Cheremisinoff, Handbook of water and wastewater treatment technology, Marcel Dekker, New York, 1995
  5. Andrzej T. Gierczycki, Łukasz Kurowski, Jan Thullie, Gas cleaning and wastewater treatment for industrial and engineering chemistry students, Wydawnictwo Politechniki Śląskiej, Gliwice, 2011
  6. Georges Guiochon, Claude L. Guillemin, Quantitative gas chromatography for laboratory analyses and on-line process control, Elsevier, Amsterdam, 1988
  7. Richard L. MacCreery, Raman spectroscopy for chemical analysis, Wiley-Interscience, New York, 2000

Treści programowe - laboratoria

KODTreść programowaGodziny
T-L-1Reaction exhaust gases – MS analysis5
T-L-2Reactivation of catalyst for ammonia synthesis5
T-L-3Activation of heterogeneous catalyst based on cobalt compounds5
T-L-4XRD phase analysis catalysts5
T-L-5SEM analysis of catalysts5
T-L-6XRF analysis of catalysts5
T-L-7Deep oxidation methods in waste water treatment5
T-L-8GC and GC-MS methods as a methods for separation and analysis5
T-L-9FTIR analysis of the products5
45

Treści programowe - wykłady

KODTreść programowaGodziny
T-W-1Instrumental methods of chemical composition analysis. Selecting of a proper analytical methods. Theoretical basics of atomic spectroscopy. Inductively Coupled Plasma, ICP. Atomic absorption spectroscopy, AAS. Molecular spectra method. Infrared Spectroscopy, FTIR, UV-VIS Spectroscopy, Raman Spectroscopy RS. X-ray methods. X-Ray Fluorescence, XRF, X-Ray Microanalysis; GC and GC-MS in separation and analysis of post-reaction mixtures.4
T-W-2Chemical analysis of the surface of solid state. Physicochemical basics of Electro-spectroscopy methods. Methods: Electron Spectroscopy for Chemical Analysis, ESCA, including X-ray Photoelectron Spectroscopy, XPS, and Ultraviolet Photoemission Spectroscopy, UPS; Auger Electron Spectroscopy, AES, Electron Energy Loss Spectroscopy.4
T-W-3Adsorption/desorption methods and temperature programmed techniques. Thermogravimetry, TG, Temperature Programmed Desorption, TPD, Temperature Programmed Oxidation, TPO, Temperature Programmed Reduction, TPR, Temperature Programmed Surface Reaction, TPSR. Mass spectrometry.3
T-W-4Analysis of phase composition, structure and topography. X-Ray Diffraction, XRD, Reflection High Energy Electron Diffraction, RHEED, Low Energy Electron Diffraction, LEED. Mössbauer Spectroscopy. Scanning Electron Microscopy, SEM, and Transmission Electron Microscopy, TEM, Atomic Force Microscopy, AFM.4
15

Formy aktywności - laboratoria

KODForma aktywnościGodziny
A-L-1Participation in laboratory classes45
A-L-2Data evaluation and preparation of raports28
A-L-3Consultations2
75
(*) 1 punkt ECTS, odpowiada około 30 godzinom aktywności studenta

Formy aktywności - wykłady

KODForma aktywnościGodziny
A-W-1Obligatory attendance the lactures15
A-W-2Repetition of the material8
A-W-3Consultations2
25
(*) 1 punkt ECTS, odpowiada około 30 godzinom aktywności studenta
PoleKODZnaczenie kodu
Zamierzone efekty uczenia sięChEn_1A_C09b_W01Student knows theory required to design basic chemical technology process in laboratory scale.
Odniesienie do efektów kształcenia dla kierunku studiówChEn_1A_W07Has systematic, theory-based general knowledge within the scope of chemical engineering and technology.
ChEn_1A_W11Has detailed knowledge within the scope of machine theory and instruments in chemical industry and related industries as well as the basics of designing instruments and processes.
ChEn_1A_W08Has systematic, theory-based knowledge of the key issues in chemical engineering and technology connected with the unit operations and processes.
ChEn_1A_W06Has basic knowledge within the scope of product and quality engineering.
Cel przedmiotuC-1Getting knowledge about analytical methods applied in Chemical Technology
Treści programoweT-W-1Instrumental methods of chemical composition analysis. Selecting of a proper analytical methods. Theoretical basics of atomic spectroscopy. Inductively Coupled Plasma, ICP. Atomic absorption spectroscopy, AAS. Molecular spectra method. Infrared Spectroscopy, FTIR, UV-VIS Spectroscopy, Raman Spectroscopy RS. X-ray methods. X-Ray Fluorescence, XRF, X-Ray Microanalysis; GC and GC-MS in separation and analysis of post-reaction mixtures.
T-W-2Chemical analysis of the surface of solid state. Physicochemical basics of Electro-spectroscopy methods. Methods: Electron Spectroscopy for Chemical Analysis, ESCA, including X-ray Photoelectron Spectroscopy, XPS, and Ultraviolet Photoemission Spectroscopy, UPS; Auger Electron Spectroscopy, AES, Electron Energy Loss Spectroscopy.
T-W-4Analysis of phase composition, structure and topography. X-Ray Diffraction, XRD, Reflection High Energy Electron Diffraction, RHEED, Low Energy Electron Diffraction, LEED. Mössbauer Spectroscopy. Scanning Electron Microscopy, SEM, and Transmission Electron Microscopy, TEM, Atomic Force Microscopy, AFM.
T-W-3Adsorption/desorption methods and temperature programmed techniques. Thermogravimetry, TG, Temperature Programmed Desorption, TPD, Temperature Programmed Oxidation, TPO, Temperature Programmed Reduction, TPR, Temperature Programmed Surface Reaction, TPSR. Mass spectrometry.
Metody nauczaniaM-1Lecture
Sposób ocenyS-1Ocena podsumowująca: Written exam
Kryteria ocenyOcenaKryterium oceny
2,0
3,0Student deliver at least 60% of correct answers
3,5
4,0
4,5
5,0
PoleKODZnaczenie kodu
Zamierzone efekty uczenia sięChEn_1A_C09b_U01Student is able to mount basic laboratory scale instalation used in chemical technology and evaluate the obtained data with mother IT tools.
Odniesienie do efektów kształcenia dla kierunku studiówChEn_1A_U01Is able to obtain information from literature, data bases and other sources related to chemical engineering and technology as well as related areas; is able to integrate the obtained information, interpret it, draw proper conclusions and formulate opinions with their justification.
ChEn_1A_U03Is able to prepare, in English or another foreign language, a well-documented study of problems within the scope of chemical and process engineering; is able to develop documentation concerning the accomplishment of an engineering task.
ChEn_1A_U05Has the ability to learn, e.g. to raise professional competences.
ChEn_1A_U08Is able to plan and conduct process experiments, including measurements and computer simulations, as well as to interpret the obtained results and draw conclusions.
ChEn_1A_U09Is able to use analytic, numerical and experimental methods to formulate and solve engineering tasks.
ChEn_1A_U16Is able to assess the usefulness of routine methods and tools used for solving a simple engineering task of practical nature characteristic for chemical engineering and technology as well as select and use a proper performance method and tools.
Cel przedmiotuC-1Getting knowledge about analytical methods applied in Chemical Technology
Treści programoweT-L-1Reaction exhaust gases – MS analysis
T-L-2Reactivation of catalyst for ammonia synthesis
T-L-3Activation of heterogeneous catalyst based on cobalt compounds
T-L-4XRD phase analysis catalysts
T-L-5SEM analysis of catalysts
T-L-6XRF analysis of catalysts
T-L-7Deep oxidation methods in waste water treatment
T-L-8GC and GC-MS methods as a methods for separation and analysis
T-L-9FTIR analysis of the products
Metody nauczaniaM-1Lecture
Sposób ocenyS-2Ocena formująca: approbation
Kryteria ocenyOcenaKryterium oceny
2,0
3,0Student is able to choose analytical method to solve specific problem
3,5
4,0
4,5
5,0
PoleKODZnaczenie kodu
Zamierzone efekty uczenia sięChEn_1A_C09b_K01Student is able to work in team in designing the chemical technology laboratory scale setups.
Odniesienie do efektów kształcenia dla kierunku studiówChEn_1A_K01Understands the need of learning and raising professional and personal competences, motivating other colleagues.
ChEn_1A_K03Is able to cooperate and work in a group. Is able to perform the function of a team leader; is able to estimate the time necessary to accomplish the assigned task.
ChEn_1A_K04Is able to determine the priorities used for performance of the tasks of his/her own or other team members in order to achieve the goal set.
ChEn_1A_K05Is able to manage his/her own professional development, taking decisions and solving problems, including interpersonal ones connected with job performance.
Cel przedmiotuC-1Getting knowledge about analytical methods applied in Chemical Technology
Treści programoweT-W-1Instrumental methods of chemical composition analysis. Selecting of a proper analytical methods. Theoretical basics of atomic spectroscopy. Inductively Coupled Plasma, ICP. Atomic absorption spectroscopy, AAS. Molecular spectra method. Infrared Spectroscopy, FTIR, UV-VIS Spectroscopy, Raman Spectroscopy RS. X-ray methods. X-Ray Fluorescence, XRF, X-Ray Microanalysis; GC and GC-MS in separation and analysis of post-reaction mixtures.
T-W-2Chemical analysis of the surface of solid state. Physicochemical basics of Electro-spectroscopy methods. Methods: Electron Spectroscopy for Chemical Analysis, ESCA, including X-ray Photoelectron Spectroscopy, XPS, and Ultraviolet Photoemission Spectroscopy, UPS; Auger Electron Spectroscopy, AES, Electron Energy Loss Spectroscopy.
T-W-4Analysis of phase composition, structure and topography. X-Ray Diffraction, XRD, Reflection High Energy Electron Diffraction, RHEED, Low Energy Electron Diffraction, LEED. Mössbauer Spectroscopy. Scanning Electron Microscopy, SEM, and Transmission Electron Microscopy, TEM, Atomic Force Microscopy, AFM.
T-W-3Adsorption/desorption methods and temperature programmed techniques. Thermogravimetry, TG, Temperature Programmed Desorption, TPD, Temperature Programmed Oxidation, TPO, Temperature Programmed Reduction, TPR, Temperature Programmed Surface Reaction, TPSR. Mass spectrometry.
Metody nauczaniaM-1Lecture
Sposób ocenyS-2Ocena formująca: approbation
Kryteria ocenyOcenaKryterium oceny
2,0
3,0Student is able to cooperate in team durign problem solving
3,5
4,0
4,5
5,0