Zachodniopomorski Uniwersytet Technologiczny w Szczecinie

Administracja Centralna Uczelni - Wymiana międzynarodowa (S1)

Sylabus przedmiotu INTRODUCTION TO ORGANIC SYNTHESIS AND PRODUCTS ANALYSIS:

Informacje podstawowe

Kierunek studiów Wymiana międzynarodowa
Forma studiów studia stacjonarne Poziom pierwszego stopnia
Tytuł zawodowy absolwenta
Obszary studiów —
Profil
Moduł —
Przedmiot INTRODUCTION TO ORGANIC SYNTHESIS AND PRODUCTS ANALYSIS
Specjalność przedmiot wspólny
Jednostka prowadząca Katedra Chemii Organicznej i Chemii Fizycznej
Nauczyciel odpowiedzialny Jacek Sośnicki <Jacek.Sosnicki@zut.edu.pl>
Inni nauczyciele
ECTS (planowane) 9,0 ECTS (formy) 9,0
Forma zaliczenia zaliczenie Język angielski
Blok obieralny — Grupa obieralna —

Formy dydaktyczne

Forma dydaktycznaKODSemestrGodzinyECTSWagaZaliczenie
wykładyW1 15 1,00,50zaliczenie
ćwiczenia audytoryjneA1 15 1,00,25zaliczenie
laboratoriaL1 60 7,00,25zaliczenie

Wymagania wstępne

KODWymaganie wstępne
W-1Basic knowledge of fundamental organic chemistry.

Cele przedmiotu

KODCel modułu/przedmiotu
C-1The student knows the basic methods for construction of a carbon skeleton of organic compounds and has the fundamental knowledge on the methods of their analyses.
C-2The student demonstrates the ability to conduct the basic organic chemistry experiments and to analyze data and results by standard analytical methods.
C-3The student knows how to carry out a basic literature search based on databases and scientific literature.
C-4The student is aware of the importance of the knowledge acquired within the subject for developement of science and for impovement of the quality of life.

Treści programowe z podziałem na formy zajęć

KODTreść programowaGodziny
ćwiczenia audytoryjne
T-A-1Exercises in planning the synthesis of organic molecules with the aid of databases.5
T-A-2Exercises in determining the structure of organic compounds by IR, NMR, MS methods.10
15
laboratoria
T-L-1Regulations and safety rules in the laboratory of organic chemistry. Basic and advanced laboratory equipment. Principles of laboratory raport preparation.5
T-L-2Preparation of Grignard reagents (Schlenk technique) and their use in organic synthesis. Synthesis of tertiary alcohol, purification by vacuum distillation, and structure analysis by IR and NMR methods.20
T-L-3Addition of C-nucleophiles to multiple carbon-carbon bonds. Eg. Addition of magnesiates to 2-pyridones. Determination of the reaction yield directly from the post-reaction mixture without isolation of the product. Isolation of the product by column chromatography and assignment its structure by IR, 1H and 13C NMR spectroscopy and MS analysis.20
T-L-4Building a carbon skeleton by using palladium catalysts. Eg. Use of Sonogashira reaction in preparation of selected alkyne product. Purification with a properly selected method. Structure analysis by spectroscopic methods.15
60
wykłady
T-W-1Databases and scientific journals as a platform to start organic synthesis.1
T-W-2Overview of IR, MS and NMR as fundamental methods for analysis of organic compounds. Practical notes.5
T-W-3Selected new and old methods for building a carbon skeleton.5
T-W-4Selected aspects of stereochemistry in organic synthesis2
T-W-5Principles of planning the synthesis of complex molecules.1
T-W-6Test.1
15

Obciążenie pracą studenta - formy aktywności

KODForma aktywnościGodziny
ćwiczenia audytoryjne
A-A-1Participation in the clasess.15
A-A-2Self-improvement in solving additional structural problems.5
A-A-3Conslutations.5
25
laboratoria
A-L-1Participation in the laboratory classes.60
A-L-2Individual literature studies.35
A-L-3Consultations.10
A-L-4Preparations for the classes.60
A-L-5Preparations of the written raports10
175
wykłady
A-W-1Participationn in the lectures.15
A-W-2Self study of recomended literature.8
A-W-3Consultations.2
25

Metody nauczania / narzędzia dydaktyczne

KODMetoda nauczania / narzędzie dydaktyczne
M-1Lecture with discussion.
M-2Laboratory exercises.
M-3Classes with discussion.

Sposoby oceny

KODSposób oceny
S-1Ocena podsumowująca: Continuous assessment: laboratory reports and activity.
S-2Ocena podsumowująca: Writting the final test.

Zamierzone efekty uczenia się - wiedza

Zamierzone efekty uczenia sięOdniesienie do efektów kształcenia dla kierunku studiówOdniesienie do efektów zdefiniowanych dla obszaru kształceniaCel przedmiotuTreści programoweMetody nauczaniaSposób oceny
WM-WTiICh_1-_??_W01
The studen has basic knowledge on structure, reactivity of simple organic compounds and on basic methods of their analyses.		——C-1T-W-1, T-W-2, T-W-3, T-W-4, T-W-5, T-A-1, T-A-2, T-L-2, T-L-3, T-L-4M-1, M-2, M-3S-2

Zamierzone efekty uczenia się - umiejętności

Zamierzone efekty uczenia sięOdniesienie do efektów kształcenia dla kierunku studiówOdniesienie do efektów zdefiniowanych dla obszaru kształceniaCel przedmiotuTreści programoweMetody nauczaniaSposób oceny
WM-WTiICh_1-_??_U01
The studen is able to plan and perform basic synthetic transformations on the basis of informations taken from databases and scientific literature and is able to analyse the products by using basic analytical methods.		——C-2, C-3T-W-1, T-W-2, T-W-3, T-W-4, T-W-5, T-A-1, T-A-2, T-L-1, T-L-2, T-L-3, T-L-4M-2, M-3S-1, S-2
WM-WTiICh_1-_??_U02
The studen is able to prepare the basic laboratory raport.		——C-2T-L-1, T-L-2, T-L-3, T-L-4M-2S-1

Zamierzone efekty uczenia się - inne kompetencje społeczne i personalne

Zamierzone efekty uczenia sięOdniesienie do efektów kształcenia dla kierunku studiówOdniesienie do efektów zdefiniowanych dla obszaru kształceniaCel przedmiotuTreści programoweMetody nauczaniaSposób oceny
WM-WTiICh_1-_??_K01
The student is aware of the importance of organic chemistry in life and science.		——C-4T-W-1, T-W-2, T-W-3, T-W-4, T-W-5, T-A-1, T-A-2, T-L-1, T-L-2, T-L-3, T-L-4M-1, M-2, M-3S-1, S-2

Kryterium oceny - wiedza

Efekt uczenia sięOcenaKryterium oceny
WM-WTiICh_1-_??_W01
The studen has basic knowledge on structure, reactivity of simple organic compounds and on basic methods of their analyses.		2,0
3,0Positive grade of the final test (more than 55% correct answers)
3,5
4,0
4,5
5,0

Kryterium oceny - umiejętności

Efekt uczenia sięOcenaKryterium oceny
WM-WTiICh_1-_??_U01
The studen is able to plan and perform basic synthetic transformations on the basis of informations taken from databases and scientific literature and is able to analyse the products by using basic analytical methods.		2,0
3,0Positive grades of lab. raports.
3,5
4,0
4,5
5,0
WM-WTiICh_1-_??_U02
The studen is able to prepare the basic laboratory raport.		2,0
3,0Positive grades of lab. raports.
3,5
4,0
4,5
5,0

Kryterium oceny - inne kompetencje społeczne i personalne

Efekt uczenia sięOcenaKryterium oceny
WM-WTiICh_1-_??_K01
The student is aware of the importance of organic chemistry in life and science.		2,0
3,0Positive grade of the final test (more than 55% correct answers) and positive grades of lab. raports.
3,5
4,0
4,5
5,0

Literatura podstawowa

  1. J. J. Li, C. Limberakis, D. A. Pflum, Modern Organic Synthesis in the laboratory. A collection of standard experimental procedures, OXFORD University Press, 2007
  2. John McMurry, Organic Chemistry, Brooks/Cole, 2012, 8e

Literatura dodatkowa

  1. Clayden, Greeves, Warren, Wothers, Organic Chemistry, Oxford, 2004

Treści programowe - ćwiczenia audytoryjne

KODTreść programowaGodziny
T-A-1Exercises in planning the synthesis of organic molecules with the aid of databases.5
T-A-2Exercises in determining the structure of organic compounds by IR, NMR, MS methods.10
15

Treści programowe - laboratoria

KODTreść programowaGodziny
T-L-1Regulations and safety rules in the laboratory of organic chemistry. Basic and advanced laboratory equipment. Principles of laboratory raport preparation.5
T-L-2Preparation of Grignard reagents (Schlenk technique) and their use in organic synthesis. Synthesis of tertiary alcohol, purification by vacuum distillation, and structure analysis by IR and NMR methods.20
T-L-3Addition of C-nucleophiles to multiple carbon-carbon bonds. Eg. Addition of magnesiates to 2-pyridones. Determination of the reaction yield directly from the post-reaction mixture without isolation of the product. Isolation of the product by column chromatography and assignment its structure by IR, 1H and 13C NMR spectroscopy and MS analysis.20
T-L-4Building a carbon skeleton by using palladium catalysts. Eg. Use of Sonogashira reaction in preparation of selected alkyne product. Purification with a properly selected method. Structure analysis by spectroscopic methods.15
60

Treści programowe - wykłady

KODTreść programowaGodziny
T-W-1Databases and scientific journals as a platform to start organic synthesis.1
T-W-2Overview of IR, MS and NMR as fundamental methods for analysis of organic compounds. Practical notes.5
T-W-3Selected new and old methods for building a carbon skeleton.5
T-W-4Selected aspects of stereochemistry in organic synthesis2
T-W-5Principles of planning the synthesis of complex molecules.1
T-W-6Test.1
15

Formy aktywności - ćwiczenia audytoryjne

KODForma aktywnościGodziny
A-A-1Participation in the clasess.15
A-A-2Self-improvement in solving additional structural problems.5
A-A-3Conslutations.5
25
(*) 1 punkt ECTS, odpowiada około 30 godzinom aktywności studenta

Formy aktywności - laboratoria

KODForma aktywnościGodziny
A-L-1Participation in the laboratory classes.60
A-L-2Individual literature studies.35
A-L-3Consultations.10
A-L-4Preparations for the classes.60
A-L-5Preparations of the written raports10
175
(*) 1 punkt ECTS, odpowiada około 30 godzinom aktywności studenta

Formy aktywności - wykłady

KODForma aktywnościGodziny
A-W-1Participationn in the lectures.15
A-W-2Self study of recomended literature.8
A-W-3Consultations.2
25
(*) 1 punkt ECTS, odpowiada około 30 godzinom aktywności studenta
PoleKODZnaczenie kodu
Zamierzone efekty uczenia sięWM-WTiICh_1-_??_W01The studen has basic knowledge on structure, reactivity of simple organic compounds and on basic methods of their analyses.
Cel przedmiotuC-1The student knows the basic methods for construction of a carbon skeleton of organic compounds and has the fundamental knowledge on the methods of their analyses.
Treści programoweT-W-1Databases and scientific journals as a platform to start organic synthesis.
T-W-2Overview of IR, MS and NMR as fundamental methods for analysis of organic compounds. Practical notes.
T-W-3Selected new and old methods for building a carbon skeleton.
T-W-4Selected aspects of stereochemistry in organic synthesis
T-W-5Principles of planning the synthesis of complex molecules.
T-A-1Exercises in planning the synthesis of organic molecules with the aid of databases.
T-A-2Exercises in determining the structure of organic compounds by IR, NMR, MS methods.
T-L-2Preparation of Grignard reagents (Schlenk technique) and their use in organic synthesis. Synthesis of tertiary alcohol, purification by vacuum distillation, and structure analysis by IR and NMR methods.
T-L-3Addition of C-nucleophiles to multiple carbon-carbon bonds. Eg. Addition of magnesiates to 2-pyridones. Determination of the reaction yield directly from the post-reaction mixture without isolation of the product. Isolation of the product by column chromatography and assignment its structure by IR, 1H and 13C NMR spectroscopy and MS analysis.
T-L-4Building a carbon skeleton by using palladium catalysts. Eg. Use of Sonogashira reaction in preparation of selected alkyne product. Purification with a properly selected method. Structure analysis by spectroscopic methods.
Metody nauczaniaM-1Lecture with discussion.
M-2Laboratory exercises.
M-3Classes with discussion.
Sposób ocenyS-2Ocena podsumowująca: Writting the final test.
Kryteria ocenyOcenaKryterium oceny
2,0
3,0Positive grade of the final test (more than 55% correct answers)
3,5
4,0
4,5
5,0
PoleKODZnaczenie kodu
Zamierzone efekty uczenia sięWM-WTiICh_1-_??_U01The studen is able to plan and perform basic synthetic transformations on the basis of informations taken from databases and scientific literature and is able to analyse the products by using basic analytical methods.
Cel przedmiotuC-2The student demonstrates the ability to conduct the basic organic chemistry experiments and to analyze data and results by standard analytical methods.
C-3The student knows how to carry out a basic literature search based on databases and scientific literature.
Treści programoweT-W-1Databases and scientific journals as a platform to start organic synthesis.
T-W-2Overview of IR, MS and NMR as fundamental methods for analysis of organic compounds. Practical notes.
T-W-3Selected new and old methods for building a carbon skeleton.
T-W-4Selected aspects of stereochemistry in organic synthesis
T-W-5Principles of planning the synthesis of complex molecules.
T-A-1Exercises in planning the synthesis of organic molecules with the aid of databases.
T-A-2Exercises in determining the structure of organic compounds by IR, NMR, MS methods.
T-L-1Regulations and safety rules in the laboratory of organic chemistry. Basic and advanced laboratory equipment. Principles of laboratory raport preparation.
T-L-2Preparation of Grignard reagents (Schlenk technique) and their use in organic synthesis. Synthesis of tertiary alcohol, purification by vacuum distillation, and structure analysis by IR and NMR methods.
T-L-3Addition of C-nucleophiles to multiple carbon-carbon bonds. Eg. Addition of magnesiates to 2-pyridones. Determination of the reaction yield directly from the post-reaction mixture without isolation of the product. Isolation of the product by column chromatography and assignment its structure by IR, 1H and 13C NMR spectroscopy and MS analysis.
T-L-4Building a carbon skeleton by using palladium catalysts. Eg. Use of Sonogashira reaction in preparation of selected alkyne product. Purification with a properly selected method. Structure analysis by spectroscopic methods.
Metody nauczaniaM-2Laboratory exercises.
M-3Classes with discussion.
Sposób ocenyS-1Ocena podsumowująca: Continuous assessment: laboratory reports and activity.
S-2Ocena podsumowująca: Writting the final test.
Kryteria ocenyOcenaKryterium oceny
2,0
3,0Positive grades of lab. raports.
3,5
4,0
4,5
5,0
PoleKODZnaczenie kodu
Zamierzone efekty uczenia sięWM-WTiICh_1-_??_U02The studen is able to prepare the basic laboratory raport.
Cel przedmiotuC-2The student demonstrates the ability to conduct the basic organic chemistry experiments and to analyze data and results by standard analytical methods.
Treści programoweT-L-1Regulations and safety rules in the laboratory of organic chemistry. Basic and advanced laboratory equipment. Principles of laboratory raport preparation.
T-L-2Preparation of Grignard reagents (Schlenk technique) and their use in organic synthesis. Synthesis of tertiary alcohol, purification by vacuum distillation, and structure analysis by IR and NMR methods.
T-L-3Addition of C-nucleophiles to multiple carbon-carbon bonds. Eg. Addition of magnesiates to 2-pyridones. Determination of the reaction yield directly from the post-reaction mixture without isolation of the product. Isolation of the product by column chromatography and assignment its structure by IR, 1H and 13C NMR spectroscopy and MS analysis.
T-L-4Building a carbon skeleton by using palladium catalysts. Eg. Use of Sonogashira reaction in preparation of selected alkyne product. Purification with a properly selected method. Structure analysis by spectroscopic methods.
Metody nauczaniaM-2Laboratory exercises.
Sposób ocenyS-1Ocena podsumowująca: Continuous assessment: laboratory reports and activity.
Kryteria ocenyOcenaKryterium oceny
2,0
3,0Positive grades of lab. raports.
3,5
4,0
4,5
5,0
PoleKODZnaczenie kodu
Zamierzone efekty uczenia sięWM-WTiICh_1-_??_K01The student is aware of the importance of organic chemistry in life and science.
Cel przedmiotuC-4The student is aware of the importance of the knowledge acquired within the subject for developement of science and for impovement of the quality of life.
Treści programoweT-W-1Databases and scientific journals as a platform to start organic synthesis.
T-W-2Overview of IR, MS and NMR as fundamental methods for analysis of organic compounds. Practical notes.
T-W-3Selected new and old methods for building a carbon skeleton.
T-W-4Selected aspects of stereochemistry in organic synthesis
T-W-5Principles of planning the synthesis of complex molecules.
T-A-1Exercises in planning the synthesis of organic molecules with the aid of databases.
T-A-2Exercises in determining the structure of organic compounds by IR, NMR, MS methods.
T-L-1Regulations and safety rules in the laboratory of organic chemistry. Basic and advanced laboratory equipment. Principles of laboratory raport preparation.
T-L-2Preparation of Grignard reagents (Schlenk technique) and their use in organic synthesis. Synthesis of tertiary alcohol, purification by vacuum distillation, and structure analysis by IR and NMR methods.
T-L-3Addition of C-nucleophiles to multiple carbon-carbon bonds. Eg. Addition of magnesiates to 2-pyridones. Determination of the reaction yield directly from the post-reaction mixture without isolation of the product. Isolation of the product by column chromatography and assignment its structure by IR, 1H and 13C NMR spectroscopy and MS analysis.
T-L-4Building a carbon skeleton by using palladium catalysts. Eg. Use of Sonogashira reaction in preparation of selected alkyne product. Purification with a properly selected method. Structure analysis by spectroscopic methods.
Metody nauczaniaM-1Lecture with discussion.
M-2Laboratory exercises.
M-3Classes with discussion.
Sposób ocenyS-1Ocena podsumowująca: Continuous assessment: laboratory reports and activity.
S-2Ocena podsumowująca: Writting the final test.
Kryteria ocenyOcenaKryterium oceny
2,0
3,0Positive grade of the final test (more than 55% correct answers) and positive grades of lab. raports.
3,5
4,0
4,5
5,0