Zachodniopomorski Uniwersytet Technologiczny w Szczecinie

Wydział Technologii i Inżynierii Chemicznej - Chemical Engineering (S2)
specjalność: Modern and Green Chemical Engineering

Sylabus przedmiotu Advanced Topics in Sustainable Catalysis:

Informacje podstawowe

Kierunek studiów Chemical Engineering
Forma studiów studia stacjonarne Poziom drugiego stopnia
Tytuł zawodowy absolwenta magister inżynier
Obszary studiów charakterystyki PRK, kompetencje inżynierskie PRK
Profil ogólnoakademicki
Moduł
Przedmiot Advanced Topics in Sustainable Catalysis
Specjalność Modern and Green Chemical Engineering
Jednostka prowadząca Katedra Technologii Chemicznej Organicznej i Materiałów Polimerowych
Nauczyciel odpowiedzialny Ewa Janus <Ewa.Janus@zut.edu.pl>
Inni nauczyciele
ECTS (planowane) 2,0 ECTS (formy) 2,0
Forma zaliczenia zaliczenie Język angielski
Blok obieralny Grupa obieralna

Formy dydaktyczne

Forma dydaktycznaKODSemestrGodzinyECTSWagaZaliczenie
laboratoriaL2 15 1,00,50zaliczenie
wykładyW2 15 1,00,50zaliczenie

Wymagania wstępne

KODWymaganie wstępne
W-1fundamentals of inorganic and organic chemistry

Cele przedmiotu

KODCel modułu/przedmiotu
C-1student has knowledge of the methods of catalysts immobilization and heterogenization for the purpose their recycling and multiple use in the processes of organic technology
C-2student has knowledge of lignocellulosic biomass conversion to valuable chemical products
C-3student is able to propose and carry out physical and chemical immobilization of selected catalysts on a solid support or in an ionic liquid

Treści programowe z podziałem na formy zajęć

KODTreść programowaGodziny
laboratoria
T-L-1Immobilization of metal catalysts in ionic liquids and use in chosen reaction (cycloaddition, epoxidation)5
T-L-2Heterogenization of metal catalysts and use in the chosen reaction (hydroformylation, oxidation, esterification)5
T-L-3Modification of supports and heterogeneous catalyst by ionic liquids and chosen organic transformation5
15
wykłady
T-W-1Homogenous and liquid-liquid biphasic catalysis and catalyst immobilization with ionic liquids - examples of catalytic reactions2
T-W-2Catalyst heterogenization methods for fine chemicals production - catalysts based on platinum group metals, mainly Pd, Rh, Ru, Pt catalysts3
T-W-3Synthetic strategies according to the type of interaction between the support and the active catalyst, support-metal or support - ligand interactions2
T-W-4Modification of supports and heterogeneous catalysts by Ionic Liquids: Supported Ionic Liquid Phase (SILP) and Solid Catalyst with an Ionic Liquid Layer (SCILL) Systems; transition metal catalysed transformations in SILP and SCILL systems: hydroformylation, hydrogenation, oxidation, various carbonylation, Lewis acid catalyzed alkylation3
T-W-5Asymmetric catalysis by heterogenized chiral metal complexes - industrial aspects of fine chemicals production with examples of commercialised processes2
T-W-6Catalytic dissolution and degradation of lignocellulosic biomass; acidic degradation of lignine and cellulose; transformation of lignine/cellulose depolymerization products into valuable chemicals; enzymatic processes in ionic liquids - activation and stabilization of enzymes in ILs2
T-W-7written test1
15

Obciążenie pracą studenta - formy aktywności

KODForma aktywnościGodziny
laboratoria
A-L-1attendance at labs15
A-L-2preparation of labs reports4
A-L-3preparation for the implementation of the experiment in the laboratory and the study of the necessary literature6
25
wykłady
A-W-1attendance at lectures15
A-W-2preparation for the written test9
A-W-3Consultation1
25

Metody nauczania / narzędzia dydaktyczne

KODMetoda nauczania / narzędzie dydaktyczne
M-1lecture with discussion
M-2Laboratory - practical classes

Sposoby oceny

KODSposób oceny
S-1Ocena podsumowująca: test after lectures
S-2Ocena podsumowująca: continuous assesment of student activity and laboratory report

Zamierzone efekty uczenia się - wiedza

Zamierzone efekty uczenia sięOdniesienie do efektów kształcenia dla kierunku studiówOdniesienie do efektów zdefiniowanych dla obszaru kształceniaOdniesienie do efektów uczenia się prowadzących do uzyskania tytułu zawodowego inżynieraCel przedmiotuTreści programoweMetody nauczaniaSposób oceny
ChEn_2A_C07_W01
graduate lists, describes and explains the methods of immobilization and heterogenization of catalyst and chemical technology processes of their use
ChEn_2A_W03, ChEn_2A_W04C-1T-W-1, T-W-2, T-W-3, T-W-4, T-W-5M-1S-1
ChEn_2A_C07_W02
graduate characterizes, explains, and describes degradation methods (chemical, enzymatic processes) of lignocellulosic raw materials and their usefulness for the synthesis of important chemical products
ChEn_2A_W03C-2T-W-6M-1S-1

Zamierzone efekty uczenia się - umiejętności

Zamierzone efekty uczenia sięOdniesienie do efektów kształcenia dla kierunku studiówOdniesienie do efektów zdefiniowanych dla obszaru kształceniaOdniesienie do efektów uczenia się prowadzących do uzyskania tytułu zawodowego inżynieraCel przedmiotuTreści programoweMetody nauczaniaSposób oceny
ChEn_2A_C07_U01
graduate is able to select and perform immobilization and heterogenization of catalysts and use them in chemical processes
ChEn_2A_U03, ChEn_2A_U08C-3T-L-1, T-L-2, T-L-3M-2S-2

Kryterium oceny - wiedza

Efekt uczenia sięOcenaKryterium oceny
ChEn_2A_C07_W01
graduate lists, describes and explains the methods of immobilization and heterogenization of catalyst and chemical technology processes of their use
2,0
3,0Student lists, partly correctly explains immobilization/ heterogenization methods of chosen type of catalysts and indicates the chemical processes of their use
3,5
4,0
4,5
5,0
ChEn_2A_C07_W02
graduate characterizes, explains, and describes degradation methods (chemical, enzymatic processes) of lignocellulosic raw materials and their usefulness for the synthesis of important chemical products
2,0
3,0Student partly correctly describes some of degradation methods of lignocellulosic biomass and chemical products obtained
3,5
4,0
4,5
5,0

Kryterium oceny - umiejętności

Efekt uczenia sięOcenaKryterium oceny
ChEn_2A_C07_U01
graduate is able to select and perform immobilization and heterogenization of catalysts and use them in chemical processes
2,0
3,0student carry out the immobilization/heterogenization of the catalyst in accordance with the instructions and use it in chemical catalytic reactions, but can only partially correctly describe the principle of immobilization and to limited extent can propose other immobilization methods based on the literature
3,5
4,0
4,5
5,0

Literatura podstawowa

  1. R. A. van Santen, Modern heterogeneous catalysis, Wiley-VCH Verlag GmbH & Co. KGaA, Weinheim, Germany, 2017
  2. Shaikh, Abdullah A., Heterogeneous Catalysis, Gruyter, Walter de GmbH, 2020
  3. J. R. H. Ross, Heterogeneous Catalysis. Fundamentals and Applications, Elsevier B.V., 2012

Treści programowe - laboratoria

KODTreść programowaGodziny
T-L-1Immobilization of metal catalysts in ionic liquids and use in chosen reaction (cycloaddition, epoxidation)5
T-L-2Heterogenization of metal catalysts and use in the chosen reaction (hydroformylation, oxidation, esterification)5
T-L-3Modification of supports and heterogeneous catalyst by ionic liquids and chosen organic transformation5
15

Treści programowe - wykłady

KODTreść programowaGodziny
T-W-1Homogenous and liquid-liquid biphasic catalysis and catalyst immobilization with ionic liquids - examples of catalytic reactions2
T-W-2Catalyst heterogenization methods for fine chemicals production - catalysts based on platinum group metals, mainly Pd, Rh, Ru, Pt catalysts3
T-W-3Synthetic strategies according to the type of interaction between the support and the active catalyst, support-metal or support - ligand interactions2
T-W-4Modification of supports and heterogeneous catalysts by Ionic Liquids: Supported Ionic Liquid Phase (SILP) and Solid Catalyst with an Ionic Liquid Layer (SCILL) Systems; transition metal catalysed transformations in SILP and SCILL systems: hydroformylation, hydrogenation, oxidation, various carbonylation, Lewis acid catalyzed alkylation3
T-W-5Asymmetric catalysis by heterogenized chiral metal complexes - industrial aspects of fine chemicals production with examples of commercialised processes2
T-W-6Catalytic dissolution and degradation of lignocellulosic biomass; acidic degradation of lignine and cellulose; transformation of lignine/cellulose depolymerization products into valuable chemicals; enzymatic processes in ionic liquids - activation and stabilization of enzymes in ILs2
T-W-7written test1
15

Formy aktywności - laboratoria

KODForma aktywnościGodziny
A-L-1attendance at labs15
A-L-2preparation of labs reports4
A-L-3preparation for the implementation of the experiment in the laboratory and the study of the necessary literature6
25
(*) 1 punkt ECTS, odpowiada około 30 godzinom aktywności studenta

Formy aktywności - wykłady

KODForma aktywnościGodziny
A-W-1attendance at lectures15
A-W-2preparation for the written test9
A-W-3Consultation1
25
(*) 1 punkt ECTS, odpowiada około 30 godzinom aktywności studenta
PoleKODZnaczenie kodu
Zamierzone efekty uczenia sięChEn_2A_C07_W01graduate lists, describes and explains the methods of immobilization and heterogenization of catalyst and chemical technology processes of their use
Odniesienie do efektów kształcenia dla kierunku studiówChEn_2A_W03Graduate has deep theoretical background related to catalysis and alternative and enhanced techniques in chemical and biochemical processes as well as instrumental analytical methods applied in chemical engineering.
ChEn_2A_W04Graduate has broadened and deep knowledge about the modern and green chemical and material technologies, including advanced materials and nanomaterials technologies as well as current trends in the development of chemical industrial processes.
Cel przedmiotuC-1student has knowledge of the methods of catalysts immobilization and heterogenization for the purpose their recycling and multiple use in the processes of organic technology
Treści programoweT-W-1Homogenous and liquid-liquid biphasic catalysis and catalyst immobilization with ionic liquids - examples of catalytic reactions
T-W-2Catalyst heterogenization methods for fine chemicals production - catalysts based on platinum group metals, mainly Pd, Rh, Ru, Pt catalysts
T-W-3Synthetic strategies according to the type of interaction between the support and the active catalyst, support-metal or support - ligand interactions
T-W-4Modification of supports and heterogeneous catalysts by Ionic Liquids: Supported Ionic Liquid Phase (SILP) and Solid Catalyst with an Ionic Liquid Layer (SCILL) Systems; transition metal catalysed transformations in SILP and SCILL systems: hydroformylation, hydrogenation, oxidation, various carbonylation, Lewis acid catalyzed alkylation
T-W-5Asymmetric catalysis by heterogenized chiral metal complexes - industrial aspects of fine chemicals production with examples of commercialised processes
Metody nauczaniaM-1lecture with discussion
Sposób ocenyS-1Ocena podsumowująca: test after lectures
Kryteria ocenyOcenaKryterium oceny
2,0
3,0Student lists, partly correctly explains immobilization/ heterogenization methods of chosen type of catalysts and indicates the chemical processes of their use
3,5
4,0
4,5
5,0
PoleKODZnaczenie kodu
Zamierzone efekty uczenia sięChEn_2A_C07_W02graduate characterizes, explains, and describes degradation methods (chemical, enzymatic processes) of lignocellulosic raw materials and their usefulness for the synthesis of important chemical products
Odniesienie do efektów kształcenia dla kierunku studiówChEn_2A_W03Graduate has deep theoretical background related to catalysis and alternative and enhanced techniques in chemical and biochemical processes as well as instrumental analytical methods applied in chemical engineering.
Cel przedmiotuC-2student has knowledge of lignocellulosic biomass conversion to valuable chemical products
Treści programoweT-W-6Catalytic dissolution and degradation of lignocellulosic biomass; acidic degradation of lignine and cellulose; transformation of lignine/cellulose depolymerization products into valuable chemicals; enzymatic processes in ionic liquids - activation and stabilization of enzymes in ILs
Metody nauczaniaM-1lecture with discussion
Sposób ocenyS-1Ocena podsumowująca: test after lectures
Kryteria ocenyOcenaKryterium oceny
2,0
3,0Student partly correctly describes some of degradation methods of lignocellulosic biomass and chemical products obtained
3,5
4,0
4,5
5,0
PoleKODZnaczenie kodu
Zamierzone efekty uczenia sięChEn_2A_C07_U01graduate is able to select and perform immobilization and heterogenization of catalysts and use them in chemical processes
Odniesienie do efektów kształcenia dla kierunku studiówChEn_2A_U03Graduate is able to use broadened and deep knowledge about the modern and green chemical and material technologies as well as current trends in the development of chemical industrial processes.
ChEn_2A_U08Graduate is able to apply the principles of occupational health and safety in the laboratory.
Cel przedmiotuC-3student is able to propose and carry out physical and chemical immobilization of selected catalysts on a solid support or in an ionic liquid
Treści programoweT-L-1Immobilization of metal catalysts in ionic liquids and use in chosen reaction (cycloaddition, epoxidation)
T-L-2Heterogenization of metal catalysts and use in the chosen reaction (hydroformylation, oxidation, esterification)
T-L-3Modification of supports and heterogeneous catalyst by ionic liquids and chosen organic transformation
Metody nauczaniaM-2Laboratory - practical classes
Sposób ocenyS-2Ocena podsumowująca: continuous assesment of student activity and laboratory report
Kryteria ocenyOcenaKryterium oceny
2,0
3,0student carry out the immobilization/heterogenization of the catalyst in accordance with the instructions and use it in chemical catalytic reactions, but can only partially correctly describe the principle of immobilization and to limited extent can propose other immobilization methods based on the literature
3,5
4,0
4,5
5,0