Zachodniopomorski Uniwersytet Technologiczny w Szczecinie

Administracja Centralna Uczelni - Wymiana międzynarodowa (S2)

Sylabus przedmiotu SPECTROSCOPIC METHODS:

Informacje podstawowe

Kierunek studiów Wymiana międzynarodowa
Forma studiów studia stacjonarne Poziom drugiego stopnia
Tytuł zawodowy absolwenta
Obszary studiów
Profil
Moduł
Przedmiot SPECTROSCOPIC METHODS
Specjalność przedmiot wspólny
Jednostka prowadząca Katedra Chemii Organicznej i Chemii Fizycznej
Nauczyciel odpowiedzialny Elwira Wróblewska <Elwira.Wroblewska@zut.edu.pl>
Inni nauczyciele Elwira Wróblewska <Elwira.Wroblewska@zut.edu.pl>
ECTS (planowane) 4,0 ECTS (formy) 4,0
Forma zaliczenia zaliczenie Język angielski
Blok obieralny Grupa obieralna

Formy dydaktyczne

Forma dydaktycznaKODSemestrGodzinyECTSWagaZaliczenie
laboratoriaL1 45 2,00,31zaliczenie
wykładyW1 15 1,00,38zaliczenie
ćwiczenia audytoryjneA1 15 1,00,31zaliczenie

Wymagania wstępne

KODWymaganie wstępne
W-1Fundamentals of physical chemistry.
W-2Fundamentals of organic chemistry.

Cele przedmiotu

KODCel modułu/przedmiotu
C-1To gain the knowledge about the theory of spectroscopic methods and their application in qualitative and quantitative analysis.

Treści programowe z podziałem na formy zajęć

KODTreść programowaGodziny
ćwiczenia audytoryjne
T-A-1Calculation of a compound concentration expressed in various concentration units.2
T-A-2Calculation the concentration of a solution after dillution.2
T-A-3Solving some excercisses concerning the interaction of the matter with light (absorbance, transmitance).1
T-A-4Determination of compounds based on Lambert-Beer's low in single and multicomponent mixtures.3
T-A-5The application of calibration curve in quantitative analysis of componds.2
T-A-6Limit of detection, method sensitivity and precision - calculation.1
T-A-7The application of NMR spectroscopy in qualitative and quantitative analysis of organic compounds (the calculation of the position of the band corresponding to particular proton on the basis on empirical equations, determination of a compound purity).2
T-A-8Application of MS spectra in determination of organic compounds composition (Beynon table).2
15
laboratoria
T-L-1The measurements of UV-vis spectra and their application in qualitative and quantitative analysis of various compounds.10
T-L-2The recording and interpretation of IR spectra.10
T-L-3Analysis of multicomponent mixtures by spectroscopic methods supported by computer programs.10
T-L-4Precise analysis of NMR spectra with the use of technical software.10
T-L-5The interpretation of MS spectra of various group of organic compounds.5
45
wykłady
T-W-1Explanation of wave-particle duality of electromagnetic radiation and influence of its absorption/emission by atom or molecule on their properties. Theoretical studies of phenomena proceeding in the molecule/atom under the irradiation.2
T-W-2The theory of ultraviolet-visual spectroscopy (UV-VIS); the Lambert-Beer's low and the reason of the departure from this low: association, solvatochromism, thermochromism, photochromism, halochromism.2
T-W-3The application of UV-vis spectrophotometry to the analysis of multicomponent mixtures (theory, mathematics and software).2
T-W-4The use of UV-vis spectrophotometers into the studies of luminescent materials.1
T-W-5Infrared spectroscopy (IR) and its application to qualitative analysis of solids and liquids.2
T-W-6The application of IR spectroscopy to quantitative analysis of compounds (methods, their possibilities and limitations).2
T-W-7The theory of NMR spectrometry. The analysis of the spectra of various compounds.2
T-W-8MS spectrometry: types of MS spectrometers, the methods of ionisation.2
15

Obciążenie pracą studenta - formy aktywności

KODForma aktywnościGodziny
ćwiczenia audytoryjne
A-A-1The participation in the classes.15
A-A-2The individual preparation of student for the classes.15
30
laboratoria
A-L-1The participation in the laboratory.45
A-L-2The individual preparation of student for the laboratory.15
60
wykłady
A-W-1The participation in the lectures with the possibility of the discussion.15
A-W-2Individual studies of the subject - reading of the recomended literature.10
A-W-3Individual analysis of avialable spectra5
30

Metody nauczania / narzędzia dydaktyczne

KODMetoda nauczania / narzędzie dydaktyczne
M-1The lectures with the discussion.
M-2Classes
M-3Laboratory

Sposoby oceny

KODSposób oceny
S-1Ocena podsumowująca: Written exam and/or oral discussion
S-2Ocena formująca: Assessment of laboratory written report
S-3Ocena formująca: Assessment of homework assignments.
S-4Ocena formująca: Evaluation of the student’s work based on the student activity during the course.

Zamierzone efekty uczenia się - wiedza

Zamierzone efekty uczenia sięOdniesienie do efektów kształcenia dla kierunku studiówOdniesienie do efektów zdefiniowanych dla obszaru kształceniaCel przedmiotuTreści programoweMetody nauczaniaSposób oceny
WM_1-_??_W01
He has a knowledge about the fundamentals of the selected spectroscopic method and their application in qualitative and quantitative analysis.
C-1T-W-1, T-W-2, T-W-3, T-W-4, T-W-5, T-W-6, T-W-7, T-W-8M-1S-1, S-4

Zamierzone efekty uczenia się - umiejętności

Zamierzone efekty uczenia sięOdniesienie do efektów kształcenia dla kierunku studiówOdniesienie do efektów zdefiniowanych dla obszaru kształceniaCel przedmiotuTreści programoweMetody nauczaniaSposób oceny
WM_1-_??_U01
Student is able to make some calculation concerning the analysis with the interpretation of obtained results.
C-1T-A-8, T-A-6, T-A-4, T-A-5, T-A-1, T-A-2, T-A-3, T-A-7M-2, M-3S-2, S-3
WM_1-_??_U02
Student can plane and carry the experiment with the interpretation of obtained results.
C-1T-L-1, T-L-2, T-L-3, T-L-4, T-L-5M-3S-2, S-4

Zamierzone efekty uczenia się - inne kompetencje społeczne i personalne

Zamierzone efekty uczenia sięOdniesienie do efektów kształcenia dla kierunku studiówOdniesienie do efektów zdefiniowanych dla obszaru kształceniaCel przedmiotuTreści programoweMetody nauczaniaSposób oceny
WM_1-_??_K01
Student is able to choose the appropriate method in order to solve particular problem.
C-1T-W-1, T-L-1, T-L-2, T-L-3, T-L-4, T-L-5M-3S-4

Kryterium oceny - wiedza

Efekt uczenia sięOcenaKryterium oceny
WM_1-_??_W01
He has a knowledge about the fundamentals of the selected spectroscopic method and their application in qualitative and quantitative analysis.
2,0
3,0Student has a fundamental knowledge about particular spectroscopic method.
3,5
4,0
4,5
5,0

Kryterium oceny - umiejętności

Efekt uczenia sięOcenaKryterium oceny
WM_1-_??_U01
Student is able to make some calculation concerning the analysis with the interpretation of obtained results.
2,0
3,0Student is able to make some calculation concerning the analysis.
3,5
4,0
4,5
5,0
WM_1-_??_U02
Student can plane and carry the experiment with the interpretation of obtained results.
2,0
3,0Student can carry simple experiment with the interpretation of obtained results.
3,5
4,0
4,5
5,0

Kryterium oceny - inne kompetencje społeczne i personalne

Efekt uczenia sięOcenaKryterium oceny
WM_1-_??_K01
Student is able to choose the appropriate method in order to solve particular problem.
2,0
3,0Student is able to choose the appropriate method in order to solve less complicated problem.
3,5
4,0
4,5
5,0

Literatura podstawowa

  1. Field, L. D, Strnhell, S, Kalman, J.R., Organic structures from spectra, Chichester: John Wiley and Sons, 2002
  2. Bartecki, A. , Lang, L., Absorption spectra in the ultraviolet and visible region., House of the Hungarian. Academy of Sciences, Budapest, 1982
  3. Láng, L., Holly, S, Sohár, P., Absorption spectra in the infrared region, Akadémiai Kiadó, Budapest, 1980
  4. Rahman, Atta-ur, One and two dimensional NMR spectroscopy, Elsevier, Amsterdam, 2011
  5. Perkampus, Heinz-Helmut, Encyclopedia of spectroscopy, Weinheim : VCH, 1995

Literatura dodatkowa

  1. Reichardt, Christian, Solvents and solvent effects in organic chemistry, Weinheim : VCH, 1990
  2. Evans, Myron Wyn, S., The photon’s magnetic field : optical NMR spectroscopy, World Scientific, Singapore, 1992
  3. Strobel, Howard A., Chemical instrumentation : a systematic approach to instrumental analysis, Reading, Mass. : Addison-Wesley, 2011

Treści programowe - ćwiczenia audytoryjne

KODTreść programowaGodziny
T-A-1Calculation of a compound concentration expressed in various concentration units.2
T-A-2Calculation the concentration of a solution after dillution.2
T-A-3Solving some excercisses concerning the interaction of the matter with light (absorbance, transmitance).1
T-A-4Determination of compounds based on Lambert-Beer's low in single and multicomponent mixtures.3
T-A-5The application of calibration curve in quantitative analysis of componds.2
T-A-6Limit of detection, method sensitivity and precision - calculation.1
T-A-7The application of NMR spectroscopy in qualitative and quantitative analysis of organic compounds (the calculation of the position of the band corresponding to particular proton on the basis on empirical equations, determination of a compound purity).2
T-A-8Application of MS spectra in determination of organic compounds composition (Beynon table).2
15

Treści programowe - laboratoria

KODTreść programowaGodziny
T-L-1The measurements of UV-vis spectra and their application in qualitative and quantitative analysis of various compounds.10
T-L-2The recording and interpretation of IR spectra.10
T-L-3Analysis of multicomponent mixtures by spectroscopic methods supported by computer programs.10
T-L-4Precise analysis of NMR spectra with the use of technical software.10
T-L-5The interpretation of MS spectra of various group of organic compounds.5
45

Treści programowe - wykłady

KODTreść programowaGodziny
T-W-1Explanation of wave-particle duality of electromagnetic radiation and influence of its absorption/emission by atom or molecule on their properties. Theoretical studies of phenomena proceeding in the molecule/atom under the irradiation.2
T-W-2The theory of ultraviolet-visual spectroscopy (UV-VIS); the Lambert-Beer's low and the reason of the departure from this low: association, solvatochromism, thermochromism, photochromism, halochromism.2
T-W-3The application of UV-vis spectrophotometry to the analysis of multicomponent mixtures (theory, mathematics and software).2
T-W-4The use of UV-vis spectrophotometers into the studies of luminescent materials.1
T-W-5Infrared spectroscopy (IR) and its application to qualitative analysis of solids and liquids.2
T-W-6The application of IR spectroscopy to quantitative analysis of compounds (methods, their possibilities and limitations).2
T-W-7The theory of NMR spectrometry. The analysis of the spectra of various compounds.2
T-W-8MS spectrometry: types of MS spectrometers, the methods of ionisation.2
15

Formy aktywności - ćwiczenia audytoryjne

KODForma aktywnościGodziny
A-A-1The participation in the classes.15
A-A-2The individual preparation of student for the classes.15
30
(*) 1 punkt ECTS, odpowiada około 30 godzinom aktywności studenta

Formy aktywności - laboratoria

KODForma aktywnościGodziny
A-L-1The participation in the laboratory.45
A-L-2The individual preparation of student for the laboratory.15
60
(*) 1 punkt ECTS, odpowiada około 30 godzinom aktywności studenta

Formy aktywności - wykłady

KODForma aktywnościGodziny
A-W-1The participation in the lectures with the possibility of the discussion.15
A-W-2Individual studies of the subject - reading of the recomended literature.10
A-W-3Individual analysis of avialable spectra5
30
(*) 1 punkt ECTS, odpowiada około 30 godzinom aktywności studenta
PoleKODZnaczenie kodu
Zamierzone efekty uczenia sięWM_1-_??_W01He has a knowledge about the fundamentals of the selected spectroscopic method and their application in qualitative and quantitative analysis.
Cel przedmiotuC-1To gain the knowledge about the theory of spectroscopic methods and their application in qualitative and quantitative analysis.
Treści programoweT-W-1Explanation of wave-particle duality of electromagnetic radiation and influence of its absorption/emission by atom or molecule on their properties. Theoretical studies of phenomena proceeding in the molecule/atom under the irradiation.
T-W-2The theory of ultraviolet-visual spectroscopy (UV-VIS); the Lambert-Beer's low and the reason of the departure from this low: association, solvatochromism, thermochromism, photochromism, halochromism.
T-W-3The application of UV-vis spectrophotometry to the analysis of multicomponent mixtures (theory, mathematics and software).
T-W-4The use of UV-vis spectrophotometers into the studies of luminescent materials.
T-W-5Infrared spectroscopy (IR) and its application to qualitative analysis of solids and liquids.
T-W-6The application of IR spectroscopy to quantitative analysis of compounds (methods, their possibilities and limitations).
T-W-7The theory of NMR spectrometry. The analysis of the spectra of various compounds.
T-W-8MS spectrometry: types of MS spectrometers, the methods of ionisation.
Metody nauczaniaM-1The lectures with the discussion.
Sposób ocenyS-1Ocena podsumowująca: Written exam and/or oral discussion
S-4Ocena formująca: Evaluation of the student’s work based on the student activity during the course.
Kryteria ocenyOcenaKryterium oceny
2,0
3,0Student has a fundamental knowledge about particular spectroscopic method.
3,5
4,0
4,5
5,0
PoleKODZnaczenie kodu
Zamierzone efekty uczenia sięWM_1-_??_U01Student is able to make some calculation concerning the analysis with the interpretation of obtained results.
Cel przedmiotuC-1To gain the knowledge about the theory of spectroscopic methods and their application in qualitative and quantitative analysis.
Treści programoweT-A-8Application of MS spectra in determination of organic compounds composition (Beynon table).
T-A-6Limit of detection, method sensitivity and precision - calculation.
T-A-4Determination of compounds based on Lambert-Beer's low in single and multicomponent mixtures.
T-A-5The application of calibration curve in quantitative analysis of componds.
T-A-1Calculation of a compound concentration expressed in various concentration units.
T-A-2Calculation the concentration of a solution after dillution.
T-A-3Solving some excercisses concerning the interaction of the matter with light (absorbance, transmitance).
T-A-7The application of NMR spectroscopy in qualitative and quantitative analysis of organic compounds (the calculation of the position of the band corresponding to particular proton on the basis on empirical equations, determination of a compound purity).
Metody nauczaniaM-2Classes
M-3Laboratory
Sposób ocenyS-2Ocena formująca: Assessment of laboratory written report
S-3Ocena formująca: Assessment of homework assignments.
Kryteria ocenyOcenaKryterium oceny
2,0
3,0Student is able to make some calculation concerning the analysis.
3,5
4,0
4,5
5,0
PoleKODZnaczenie kodu
Zamierzone efekty uczenia sięWM_1-_??_U02Student can plane and carry the experiment with the interpretation of obtained results.
Cel przedmiotuC-1To gain the knowledge about the theory of spectroscopic methods and their application in qualitative and quantitative analysis.
Treści programoweT-L-1The measurements of UV-vis spectra and their application in qualitative and quantitative analysis of various compounds.
T-L-2The recording and interpretation of IR spectra.
T-L-3Analysis of multicomponent mixtures by spectroscopic methods supported by computer programs.
T-L-4Precise analysis of NMR spectra with the use of technical software.
T-L-5The interpretation of MS spectra of various group of organic compounds.
Metody nauczaniaM-3Laboratory
Sposób ocenyS-2Ocena formująca: Assessment of laboratory written report
S-4Ocena formująca: Evaluation of the student’s work based on the student activity during the course.
Kryteria ocenyOcenaKryterium oceny
2,0
3,0Student can carry simple experiment with the interpretation of obtained results.
3,5
4,0
4,5
5,0
PoleKODZnaczenie kodu
Zamierzone efekty uczenia sięWM_1-_??_K01Student is able to choose the appropriate method in order to solve particular problem.
Cel przedmiotuC-1To gain the knowledge about the theory of spectroscopic methods and their application in qualitative and quantitative analysis.
Treści programoweT-W-1Explanation of wave-particle duality of electromagnetic radiation and influence of its absorption/emission by atom or molecule on their properties. Theoretical studies of phenomena proceeding in the molecule/atom under the irradiation.
T-L-1The measurements of UV-vis spectra and their application in qualitative and quantitative analysis of various compounds.
T-L-2The recording and interpretation of IR spectra.
T-L-3Analysis of multicomponent mixtures by spectroscopic methods supported by computer programs.
T-L-4Precise analysis of NMR spectra with the use of technical software.
T-L-5The interpretation of MS spectra of various group of organic compounds.
Metody nauczaniaM-3Laboratory
Sposób ocenyS-4Ocena formująca: Evaluation of the student’s work based on the student activity during the course.
Kryteria ocenyOcenaKryterium oceny
2,0
3,0Student is able to choose the appropriate method in order to solve less complicated problem.
3,5
4,0
4,5
5,0