Zachodniopomorski Uniwersytet Technologiczny w Szczecinie

Administracja Centralna Uczelni - Wymiana międzynarodowa (S2)

Sylabus przedmiotu Instrumental analysis in chemical engineering:

Informacje podstawowe

Kierunek studiów Wymiana międzynarodowa
Forma studiów studia stacjonarne Poziom drugiego stopnia
Tytuł zawodowy absolwenta
Obszary studiów
Profil
Moduł
Przedmiot Instrumental analysis in chemical engineering
Specjalność przedmiot wspólny
Jednostka prowadząca Katedra Chemii Nieorganicznej i Analitycznej
Nauczyciel odpowiedzialny Piotr Tabero <Piotr.Tabero@zut.edu.pl>
Inni nauczyciele Monika Bosacka <Monika.Bosacka@zut.edu.pl>, Anna Błońska-Tabero <Anna.Blonska-Tabero@zut.edu.pl>, Grażyna Dąbrowska <Grazyna.Dabrowska@zut.edu.pl>, Elżbieta Filipek <Elzbieta.Filipek@zut.edu.pl>, Piotr Tabero <Piotr.Tabero@zut.edu.pl>, Elżbieta Tomaszewicz <Elzbieta.Tomaszewicz@zut.edu.pl>
ECTS (planowane) 4,0 ECTS (formy) 4,0
Forma zaliczenia zaliczenie Język polski
Blok obieralny Grupa obieralna

Formy dydaktyczne

Forma dydaktycznaKODSemestrGodzinyECTSWagaZaliczenie
wykładyW1 30 2,00,50zaliczenie
ćwiczenia audytoryjneA1 30 2,00,50zaliczenie

Wymagania wstępne

KODWymaganie wstępne
W-1Fundamentals of mathematics, physics and chemistry

Cele przedmiotu

KODCel modułu/przedmiotu
C-1To acqaint students with the selected instrumental methods frequently applied in industry and laboratories for identification of raw materials and products as well as for determination of their crucial properties.
C-2To teach students how to choose proper analytical method to obtain certain research goal.
C-3To teach students how to use data gained from measurements, available data bases and literature

Treści programowe z podziałem na formy zajęć

KODTreść programowaGodziny
ćwiczenia audytoryjne
T-A-1Sieve analysis. Standards. Sieving with test sieves. Microscopic determination of size and shape of grains. Microscopic inspection of quality of test sieves. Metallographic inspection of alloys.4
T-A-2Definition of crystalline solid. Morphology of crystals. Analysis and description of crystal, single crystal, twinns, policrystalline substance, amorphous substance, gravel, sand, silt, mineral and rock. Powder X-ray diffraction. X-ray phase analysis. Identification of metals and alloys. Identyfication of minerals, and components of rocks and sands from different locations.4
T-A-3Indexation of powder diffraction patterns. Determination of lattice parameters. Measurement of density using pycnometric and buoyancy methods. Rentgenographic density.4
T-A-4XRD quantitative phase analysis. Determination of grain size and lattice distortions.4
T-A-5High-temperature XRD measurements. Determination of coefficients of thermal expansion. Anisotrophy of thermal expansion. Investigations of polymorphic phase transitions.2
T-A-6Thermal analysis. Identyfication and characterization of raw materials and products of chemical industry by using DTA-TGA methods. Determination of coefficients of thermal expansion by using dilatometric method. Determiantion of thermal stability of substances and sorption properties of molecular sieves.4
T-A-7Application of IR, NIR and UV-Vis methods for identification of substances and coordination polyhedra building of their structures. Detection of small amounts of contaminants and ions with the help of UV-Vis and AAS.4
T-A-8Identification and determination of properties of precious metals and precious stones by using XRD, IR, NIR, UV-Vis and density measurements. Identification of counterfeit coins and simulants of precious stones.4
30
wykłady
T-W-1What are the instrumental analytical methods ? Classification of analytical methods.Choosing an analytical method.2
T-W-2Physical properties of substances. Measurements of density of solids and liquids.2
T-W-3Optical microscopy versus electron microscopy. Microscope solutions for metallography.2
T-W-4Crystal, single crystal, gravel, sand, silt. Grain size and shape measurement methods. Sieve analysis.2
T-W-5X-rays and their properties. X-ray fluorescence spectroscopy XRF .2
T-W-6X-ray diffraction XRD and powder X-ray diffraction. X-ray qualitative phase analysis.2
T-W-7Indexation of powder diffraction patterns and determination of lattice parameters. Diffractometric method of grain size and lattice distortion determination.2
T-W-8High-temperature, low-temperature and high-pressure rentgenographic measurements. Investigations of thermal expansion .2
T-W-9Rengenographic investigations of metals and alloys, solid solutions, nanocrystaline, semicrystalline and amorphous materials.2
T-W-10Thermal analyasis. DTA, TGA and DSC methods.2
T-W-11Dilatometric measurements of thermal expansion. Determination of thermal stability of substances and sorption properties of molecular sieves.2
T-W-12IR and NIR spectroscopic methods. Thermography.2
T-W-13UV-Vis spectroscopy. IR, UV-Vis-NIR methods for identification of substances and detection of small amounts of contaminants.2
T-W-14Atomic absorption spectrposcopy AAS.2
T-W-15The final written exam.2
30

Obciążenie pracą studenta - formy aktywności

KODForma aktywnościGodziny
ćwiczenia audytoryjne
A-A-1Participation inworkshop30
A-A-2Participation in consultations2
A-A-3Self-study of literature16
A-A-4Preparation of written reports12
60
wykłady
A-W-1Participation in lectures28
A-W-2Participation in consultations2
A-W-3Self-study of literature14
A-W-4Preparing to pass wrriten exam based on the indicated literature and other sources of knowledge14
A-W-5Finnal written exam2
60

Metody nauczania / narzędzia dydaktyczne

KODMetoda nauczania / narzędzie dydaktyczne
M-1Informative lecture with multimedia instruments, explanation
M-2Work with computers and and dedicated software.

Sposoby oceny

KODSposób oceny
S-1Ocena formująca: Final written exam
S-2Ocena formująca: Written reports.

Zamierzone efekty kształcenia - wiedza

Zamierzone efekty kształceniaOdniesienie do efektów kształcenia dla kierunku studiówOdniesienie do efektów zdefiniowanych dla obszaru kształceniaCel przedmiotuTreści programoweMetody nauczaniaSposób oceny
WM-WTiICh_2-_??_W01
Student knows physical properties of substances and terminology associated with analytical methods.
WM-WTiICh_2-_??_W02
Student knows construction and operation techniques of equipment used for identification of substances and determination of their properties

Zamierzone efekty kształcenia - umiejętności

Zamierzone efekty kształceniaOdniesienie do efektów kształcenia dla kierunku studiówOdniesienie do efektów zdefiniowanych dla obszaru kształceniaCel przedmiotuTreści programoweMetody nauczaniaSposób oceny
WM-WTiICh_2-_??_U01
Student can choose proper research method to obtain a certain research goal
WM-WTiICh_2-_??_U02
Student knows how to explain the data obtained and the phenomena exhibited in the materials analysis, knows how to design studies and elaborate results

Zamierzone efekty kształcenia - inne kompetencje społeczne i personalne

Zamierzone efekty kształceniaOdniesienie do efektów kształcenia dla kierunku studiówOdniesienie do efektów zdefiniowanych dla obszaru kształceniaCel przedmiotuTreści programoweMetody nauczaniaSposób oceny
WM-WTiICh_2-_??_K01
Student knows safety procedures for analytical equipment and understands importance of permanent learning to improve personal competencies

Literatura podstawowa

  1. C. Giacovazzo, H. Z. Monaco, D. Biterbo, F. Scordari, G. Gilli, G. Zanotti, M. Catt, Fundamentals of Crystallography, IUCR, Oxford University Press, Oxford, 2000
  2. B. D. Cullity, Elements of X-ray Diffraction, Addison-Wesley Publishing Company, Inc., London, 1978
  3. A. Gaunier, X-ray Diffraction in Crystals, Imperfect Crystals, and Amorphous Bodies, Courier Corporation, New York, 1994
  4. A. AUTHIER, G. CHAPUIS, EDS, A LITTLE DICTIONARY OF CRYSTALLOGRAPHY, INTERNATIONAL UNION OF CRYSTALLOGRAPHY, 2017, 2ND EDITION
  5. D. A. Skoog, F. J. Holler, S. R. Crouch, Principles of Instrumental Analysis, Brooks Cole, 2006, 6-th Edition
  6. S. Petrozz, Practical Instrumental Analysis: Methods, Quality Assurance and Laboratory Management, Wiley, 2012
  7. M. Granger, Instrumental Analysis, Revised Edition, Revised Updated Edition, Oxford University Press, Oxford, 2013
  8. J. Śestak, Heat, Thermal Analysis and Society, Nukleus HK, Hradec Kralove, 2004
  9. P. Gabbott Ed., Principles and Applications of Thermal Analysis, Wiley, 2008
  10. S. Franca, L. M. L. Nollet, Spectroscopic methods In Food Analysis, CRC Press, 2018

Literatura dodatkowa

  1. International Union of Crystallography: https://www.iucr.org

Treści programowe - ćwiczenia audytoryjne

KODTreść programowaGodziny
T-A-1Sieve analysis. Standards. Sieving with test sieves. Microscopic determination of size and shape of grains. Microscopic inspection of quality of test sieves. Metallographic inspection of alloys.4
T-A-2Definition of crystalline solid. Morphology of crystals. Analysis and description of crystal, single crystal, twinns, policrystalline substance, amorphous substance, gravel, sand, silt, mineral and rock. Powder X-ray diffraction. X-ray phase analysis. Identification of metals and alloys. Identyfication of minerals, and components of rocks and sands from different locations.4
T-A-3Indexation of powder diffraction patterns. Determination of lattice parameters. Measurement of density using pycnometric and buoyancy methods. Rentgenographic density.4
T-A-4XRD quantitative phase analysis. Determination of grain size and lattice distortions.4
T-A-5High-temperature XRD measurements. Determination of coefficients of thermal expansion. Anisotrophy of thermal expansion. Investigations of polymorphic phase transitions.2
T-A-6Thermal analysis. Identyfication and characterization of raw materials and products of chemical industry by using DTA-TGA methods. Determination of coefficients of thermal expansion by using dilatometric method. Determiantion of thermal stability of substances and sorption properties of molecular sieves.4
T-A-7Application of IR, NIR and UV-Vis methods for identification of substances and coordination polyhedra building of their structures. Detection of small amounts of contaminants and ions with the help of UV-Vis and AAS.4
T-A-8Identification and determination of properties of precious metals and precious stones by using XRD, IR, NIR, UV-Vis and density measurements. Identification of counterfeit coins and simulants of precious stones.4
30

Treści programowe - wykłady

KODTreść programowaGodziny
T-W-1What are the instrumental analytical methods ? Classification of analytical methods.Choosing an analytical method.2
T-W-2Physical properties of substances. Measurements of density of solids and liquids.2
T-W-3Optical microscopy versus electron microscopy. Microscope solutions for metallography.2
T-W-4Crystal, single crystal, gravel, sand, silt. Grain size and shape measurement methods. Sieve analysis.2
T-W-5X-rays and their properties. X-ray fluorescence spectroscopy XRF .2
T-W-6X-ray diffraction XRD and powder X-ray diffraction. X-ray qualitative phase analysis.2
T-W-7Indexation of powder diffraction patterns and determination of lattice parameters. Diffractometric method of grain size and lattice distortion determination.2
T-W-8High-temperature, low-temperature and high-pressure rentgenographic measurements. Investigations of thermal expansion .2
T-W-9Rengenographic investigations of metals and alloys, solid solutions, nanocrystaline, semicrystalline and amorphous materials.2
T-W-10Thermal analyasis. DTA, TGA and DSC methods.2
T-W-11Dilatometric measurements of thermal expansion. Determination of thermal stability of substances and sorption properties of molecular sieves.2
T-W-12IR and NIR spectroscopic methods. Thermography.2
T-W-13UV-Vis spectroscopy. IR, UV-Vis-NIR methods for identification of substances and detection of small amounts of contaminants.2
T-W-14Atomic absorption spectrposcopy AAS.2
T-W-15The final written exam.2
30

Formy aktywności - ćwiczenia audytoryjne

KODForma aktywnościGodziny
A-A-1Participation inworkshop30
A-A-2Participation in consultations2
A-A-3Self-study of literature16
A-A-4Preparation of written reports12
60
(*) 1 punkt ECTS, odpowiada około 30 godzinom aktywności studenta

Formy aktywności - wykłady

KODForma aktywnościGodziny
A-W-1Participation in lectures28
A-W-2Participation in consultations2
A-W-3Self-study of literature14
A-W-4Preparing to pass wrriten exam based on the indicated literature and other sources of knowledge14
A-W-5Finnal written exam2
60
(*) 1 punkt ECTS, odpowiada około 30 godzinom aktywności studenta
PoleKODZnaczenie kodu
Zamierzone efekty kształceniaWM-WTiICh_2-_??_W01Student knows physical properties of substances and terminology associated with analytical methods.
PoleKODZnaczenie kodu
Zamierzone efekty kształceniaWM-WTiICh_2-_??_W02Student knows construction and operation techniques of equipment used for identification of substances and determination of their properties
PoleKODZnaczenie kodu
Zamierzone efekty kształceniaWM-WTiICh_2-_??_U01Student can choose proper research method to obtain a certain research goal
PoleKODZnaczenie kodu
Zamierzone efekty kształceniaWM-WTiICh_2-_??_U02Student knows how to explain the data obtained and the phenomena exhibited in the materials analysis, knows how to design studies and elaborate results
PoleKODZnaczenie kodu
Zamierzone efekty kształceniaWM-WTiICh_2-_??_K01Student knows safety procedures for analytical equipment and understands importance of permanent learning to improve personal competencies