Zachodniopomorski Uniwersytet Technologiczny w Szczecinie

Administracja Centralna Uczelni - Wymiana międzynarodowa (S2)

Sylabus przedmiotu Instrumental analysis:

Informacje podstawowe

Kierunek studiów Wymiana międzynarodowa
Forma studiów studia stacjonarne Poziom drugiego stopnia
Tytuł zawodowy absolwenta
Obszary studiów
Profil
Moduł
Przedmiot Instrumental analysis
Specjalność przedmiot wspólny
Jednostka prowadząca Katedra Chemii Organicznej i Chemii Fizycznej
Nauczyciel odpowiedzialny Elwira Wróblewska <Elwira.Wroblewska@zut.edu.pl>
Inni nauczyciele Marta Sawicka <Marta.Sawicka@zut.edu.pl>, Elwira Wróblewska <Elwira.Wroblewska@zut.edu.pl>
ECTS (planowane) 4,0 ECTS (formy) 4,0
Forma zaliczenia zaliczenie Język angielski
Blok obieralny Grupa obieralna

Formy dydaktyczne

Forma dydaktycznaKODSemestrGodzinyECTSWagaZaliczenie
laboratoriaL2 45 2,00,31zaliczenie
ćwiczenia audytoryjneA2 15 1,00,31zaliczenie
wykładyW2 15 1,00,38zaliczenie

Wymagania wstępne

KODWymaganie wstępne
W-1Basis of physical chemistry, organic chemistry, general chemistry, analytical methods.

Cele przedmiotu

KODCel modułu/przedmiotu
C-1Theoretical and practical learning about instrumental methods applied in quantitative and qualitative analysis;
C-2Theoretical studies about the phenomena used in the particular method as well as practical interpretation of the results given.

Treści programowe z podziałem na formy zajęć

KODTreść programowaGodziny
ćwiczenia audytoryjne
T-A-1The ways of preparing of the solution with a given concentration.2
T-A-2The ways of expression of the content od some components of the solution.2
T-A-3Units usually used in absorption spectra.1
T-A-4The application of Lambert-Beer's low in quantitative analysis of single and multicomponent mixtures.4
T-A-5Calibration curve and their application in quantitative analysis.1
T-A-6The characteristic of the analytical method (limit of detection, method sensitivity and precision).1
T-A-7The use of NMR spectroscopy in qualitative and quantitative analysis of organic compounds.2
T-A-8The use of some information which are read off from chromatogram into qualitative and quantitative analysis of organic compounds2
15
laboratoria
T-L-1Measurements of UV-vis spectra and their application in the studies of solute-solvent intermolecular interaction , as well as in quantitative analysis.10
T-L-2The interpretation of HNMR spectra as a key to the determination of the structure of organic compounds.10
T-L-3The application of IR method in qualitative and quantitative analysis of organic compounds.10
T-L-4The application of chromatographic method in qualitative and quantitative analysis of multicomponent mixtures.10
T-L-5The determination of some metals with the use of ASA method.5
45
wykłady
T-W-1The fundamental definitions concerning analytical process, the kind of analytical method with respect to instrumental method analysis.1
T-W-2Classification of the methods of instrumental analysis, particularly spectroscopic and chromatographic ones.1
T-W-3Explanation of wave-particle duality of electromagnetic radiation and influence of its absorption/emission by atom or molecule on their properties.1
T-W-4Theoretical studies of phenomena proceeding in the molecule/atom under the irradiation and their application in particular methods i.e. ultraviolet-visual spectroscopy (UV-VIS), infrared spectroscopy (IR), nuclear magnetic resonance spectroscopy (NMR), mass spectroscopy (MS), atomic absorption spectroscopy (AAS), X-ray absorption, atomic emission spectroscopy (AES), flame photometry, inductively coupled plasma spectrometry (ICP), X-ray fluorescence (XRF), atomic fluorescence.9
T-W-5Explanation of phenomena, concepts, and definitions used in chromatographic methods. The ways of separation of a mixture components.3
15

Obciążenie pracą studenta - formy aktywności

KODForma aktywnościGodziny
ćwiczenia audytoryjne
A-A-1The participation in the classes.15
A-A-2The individual preparation of student for the classes.15
30
laboratoria
A-L-1The participation in the laboratory.45
A-L-2The individual preparation of student for the laboratory.10
A-L-3The preparation of laboratory report.5
60
wykłady
A-W-1The participation in the lectures with the possibility of the discussion.15
A-W-2Individual studies of the subject - reading of the recomended literature10
A-W-3The individual preparation of student for the exam.5
30

Metody nauczania / narzędzia dydaktyczne

KODMetoda nauczania / narzędzie dydaktyczne
M-1The lectures with the discussion.
M-2Classes
M-3Laboratory

Sposoby oceny

KODSposób oceny
S-1Ocena podsumowująca: Written exam and/or oral discussion.
S-2Ocena formująca: Assessment of laboratory written report.
S-3Ocena formująca: Assessment of homework assignments.
S-4Ocena formująca: Evaluation of the student’s work based on the student activity during the course.

Zamierzone efekty kształcenia - wiedza

Zamierzone efekty kształceniaOdniesienie do efektów kształcenia dla kierunku studiówOdniesienie do efektów zdefiniowanych dla obszaru kształceniaCel przedmiotuTreści programoweMetody nauczaniaSposób oceny
WM-WTiICh_2-_null_W01
Student knows the phenomena applied in the instrumental analysis.
C-1T-W-1, T-W-2, T-W-3, T-W-4, T-W-5M-1S-1
WM-WTiICh_2-_null_W02
He has a knowledge about the fundamentals of the selected spectroscopic and chromatographic methods.
C-1, C-2T-W-4, T-W-5M-1S-1

Zamierzone efekty kształcenia - umiejętności

Zamierzone efekty kształceniaOdniesienie do efektów kształcenia dla kierunku studiówOdniesienie do efektów zdefiniowanych dla obszaru kształceniaCel przedmiotuTreści programoweMetody nauczaniaSposób oceny
WM-WTiICh_2-_null_U01
Student is able to to plan and carry out the experiment with the interpretation of obtained results.
C-2T-A-1, T-A-2, T-A-3, T-A-4, T-A-5, T-A-6, T-A-7, T-A-8, T-L-1, T-L-2, T-L-3, T-L-4, T-L-5M-2, M-3S-2, S-3, S-4

Zamierzone efekty kształcenia - inne kompetencje społeczne i personalne

Zamierzone efekty kształceniaOdniesienie do efektów kształcenia dla kierunku studiówOdniesienie do efektów zdefiniowanych dla obszaru kształceniaCel przedmiotuTreści programoweMetody nauczaniaSposób oceny
WM-WTiICh_2-_null_K01
Student is able to choose the appropriate method in order to solve particular problem concerning qualitative and/or quantitative analysis
C-1T-L-1, T-L-2, T-L-3, T-L-4, T-L-5, T-W-4, T-W-5M-1, M-3S-4

Kryterium oceny - wiedza

Efekt kształceniaOcenaKryterium oceny
WM-WTiICh_2-_null_W01
Student knows the phenomena applied in the instrumental analysis.
2,0
3,0Student knows the fundamentals of phenomena applied in the instrumental analysis.
3,5
4,0
4,5
5,0
WM-WTiICh_2-_null_W02
He has a knowledge about the fundamentals of the selected spectroscopic and chromatographic methods.
2,0
3,0He has a knowledge about the fundamentals of a few methods of instrumental inanalysis.
3,5
4,0
4,5
5,0

Kryterium oceny - umiejętności

Efekt kształceniaOcenaKryterium oceny
WM-WTiICh_2-_null_U01
Student is able to to plan and carry out the experiment with the interpretation of obtained results.
2,0
3,0Student is able to carry out the experiment with the simple interpretation of obtained results.
3,5
4,0
4,5
5,0

Kryterium oceny - inne kompetencje społeczne i personalne

Efekt kształceniaOcenaKryterium oceny
WM-WTiICh_2-_null_K01
Student is able to choose the appropriate method in order to solve particular problem concerning qualitative and/or quantitative analysis
2,0
3,0Student is able to choose the appropriate method in order to solve the problem concerning quantitative analysis.
3,5
4,0
4,5
5,0

Literatura podstawowa

  1. J. M. Hollas, Modern spectroscopy, John Wiley, 2011
  2. L.D. Field, S. Sternhall, J.R. Kalman, Organic structures from spectra, 3rd ed., Chichester, John Wiley and Son, 2002
  3. J.R. Chapman, Practical Organic Mass Spectrometry, 2nd ed., Chichester, John Wiley and Son, 1993
  4. Ira N. Levin, Molecular spectroscopy, Wiley-Interscience, New York, 1975
  5. C. N. R. Rao, Ultra-violet and visible spectroscopy: chemical applications, 3rd ed., Butterworths, London, 1975
  6. ed. D. A. Ramsay, Spectroscopy, Butterworths; Baltimore, University Park Press, London, 1976
  7. Stefan Hüfner, Photoelectron spectroscopy: principles and applications, 2nd ed., Berlin, Springer, 1996

Literatura dodatkowa

  1. Ch. Reichardt, Solvents and solvent effects in organic chemistry, 2nd rev. and enl. ed., Weinheim, VCH, 1990
  2. Pradip K. Ghosh, Introduction to photoelectron spectroscopy, John Wiley and Sons, New York, 1983
  3. M. Slavin, Atomic absorption spectroscopy, John Wiley & Sons, New York, 1978
  4. J. Mika, T. Török, Analytical emission spectroscopy : fundamentals, Akadémiai Kiadó, Budapest, 1973
  5. Yoshito Takeuchi and Alan P. Marchand, Applications of NMR spectroscopy to problems in stereochemistry and conformational analysis, Verlag Chemie International, Deerfield Beach, Florida, 1986

Treści programowe - ćwiczenia audytoryjne

KODTreść programowaGodziny
T-A-1The ways of preparing of the solution with a given concentration.2
T-A-2The ways of expression of the content od some components of the solution.2
T-A-3Units usually used in absorption spectra.1
T-A-4The application of Lambert-Beer's low in quantitative analysis of single and multicomponent mixtures.4
T-A-5Calibration curve and their application in quantitative analysis.1
T-A-6The characteristic of the analytical method (limit of detection, method sensitivity and precision).1
T-A-7The use of NMR spectroscopy in qualitative and quantitative analysis of organic compounds.2
T-A-8The use of some information which are read off from chromatogram into qualitative and quantitative analysis of organic compounds2
15

Treści programowe - laboratoria

KODTreść programowaGodziny
T-L-1Measurements of UV-vis spectra and their application in the studies of solute-solvent intermolecular interaction , as well as in quantitative analysis.10
T-L-2The interpretation of HNMR spectra as a key to the determination of the structure of organic compounds.10
T-L-3The application of IR method in qualitative and quantitative analysis of organic compounds.10
T-L-4The application of chromatographic method in qualitative and quantitative analysis of multicomponent mixtures.10
T-L-5The determination of some metals with the use of ASA method.5
45

Treści programowe - wykłady

KODTreść programowaGodziny
T-W-1The fundamental definitions concerning analytical process, the kind of analytical method with respect to instrumental method analysis.1
T-W-2Classification of the methods of instrumental analysis, particularly spectroscopic and chromatographic ones.1
T-W-3Explanation of wave-particle duality of electromagnetic radiation and influence of its absorption/emission by atom or molecule on their properties.1
T-W-4Theoretical studies of phenomena proceeding in the molecule/atom under the irradiation and their application in particular methods i.e. ultraviolet-visual spectroscopy (UV-VIS), infrared spectroscopy (IR), nuclear magnetic resonance spectroscopy (NMR), mass spectroscopy (MS), atomic absorption spectroscopy (AAS), X-ray absorption, atomic emission spectroscopy (AES), flame photometry, inductively coupled plasma spectrometry (ICP), X-ray fluorescence (XRF), atomic fluorescence.9
T-W-5Explanation of phenomena, concepts, and definitions used in chromatographic methods. The ways of separation of a mixture components.3
15

Formy aktywności - ćwiczenia audytoryjne

KODForma aktywnościGodziny
A-A-1The participation in the classes.15
A-A-2The individual preparation of student for the classes.15
30
(*) 1 punkt ECTS, odpowiada około 30 godzinom aktywności studenta

Formy aktywności - laboratoria

KODForma aktywnościGodziny
A-L-1The participation in the laboratory.45
A-L-2The individual preparation of student for the laboratory.10
A-L-3The preparation of laboratory report.5
60
(*) 1 punkt ECTS, odpowiada około 30 godzinom aktywności studenta

Formy aktywności - wykłady

KODForma aktywnościGodziny
A-W-1The participation in the lectures with the possibility of the discussion.15
A-W-2Individual studies of the subject - reading of the recomended literature10
A-W-3The individual preparation of student for the exam.5
30
(*) 1 punkt ECTS, odpowiada około 30 godzinom aktywności studenta
PoleKODZnaczenie kodu
Zamierzone efekty kształceniaWM-WTiICh_2-_null_W01Student knows the phenomena applied in the instrumental analysis.
Cel przedmiotuC-1Theoretical and practical learning about instrumental methods applied in quantitative and qualitative analysis;
Treści programoweT-W-1The fundamental definitions concerning analytical process, the kind of analytical method with respect to instrumental method analysis.
T-W-2Classification of the methods of instrumental analysis, particularly spectroscopic and chromatographic ones.
T-W-3Explanation of wave-particle duality of electromagnetic radiation and influence of its absorption/emission by atom or molecule on their properties.
T-W-4Theoretical studies of phenomena proceeding in the molecule/atom under the irradiation and their application in particular methods i.e. ultraviolet-visual spectroscopy (UV-VIS), infrared spectroscopy (IR), nuclear magnetic resonance spectroscopy (NMR), mass spectroscopy (MS), atomic absorption spectroscopy (AAS), X-ray absorption, atomic emission spectroscopy (AES), flame photometry, inductively coupled plasma spectrometry (ICP), X-ray fluorescence (XRF), atomic fluorescence.
T-W-5Explanation of phenomena, concepts, and definitions used in chromatographic methods. The ways of separation of a mixture components.
Metody nauczaniaM-1The lectures with the discussion.
Sposób ocenyS-1Ocena podsumowująca: Written exam and/or oral discussion.
Kryteria ocenyOcenaKryterium oceny
2,0
3,0Student knows the fundamentals of phenomena applied in the instrumental analysis.
3,5
4,0
4,5
5,0
PoleKODZnaczenie kodu
Zamierzone efekty kształceniaWM-WTiICh_2-_null_W02He has a knowledge about the fundamentals of the selected spectroscopic and chromatographic methods.
Cel przedmiotuC-1Theoretical and practical learning about instrumental methods applied in quantitative and qualitative analysis;
C-2Theoretical studies about the phenomena used in the particular method as well as practical interpretation of the results given.
Treści programoweT-W-4Theoretical studies of phenomena proceeding in the molecule/atom under the irradiation and their application in particular methods i.e. ultraviolet-visual spectroscopy (UV-VIS), infrared spectroscopy (IR), nuclear magnetic resonance spectroscopy (NMR), mass spectroscopy (MS), atomic absorption spectroscopy (AAS), X-ray absorption, atomic emission spectroscopy (AES), flame photometry, inductively coupled plasma spectrometry (ICP), X-ray fluorescence (XRF), atomic fluorescence.
T-W-5Explanation of phenomena, concepts, and definitions used in chromatographic methods. The ways of separation of a mixture components.
Metody nauczaniaM-1The lectures with the discussion.
Sposób ocenyS-1Ocena podsumowująca: Written exam and/or oral discussion.
Kryteria ocenyOcenaKryterium oceny
2,0
3,0He has a knowledge about the fundamentals of a few methods of instrumental inanalysis.
3,5
4,0
4,5
5,0
PoleKODZnaczenie kodu
Zamierzone efekty kształceniaWM-WTiICh_2-_null_U01Student is able to to plan and carry out the experiment with the interpretation of obtained results.
Cel przedmiotuC-2Theoretical studies about the phenomena used in the particular method as well as practical interpretation of the results given.
Treści programoweT-A-1The ways of preparing of the solution with a given concentration.
T-A-2The ways of expression of the content od some components of the solution.
T-A-3Units usually used in absorption spectra.
T-A-4The application of Lambert-Beer's low in quantitative analysis of single and multicomponent mixtures.
T-A-5Calibration curve and their application in quantitative analysis.
T-A-6The characteristic of the analytical method (limit of detection, method sensitivity and precision).
T-A-7The use of NMR spectroscopy in qualitative and quantitative analysis of organic compounds.
T-A-8The use of some information which are read off from chromatogram into qualitative and quantitative analysis of organic compounds
T-L-1Measurements of UV-vis spectra and their application in the studies of solute-solvent intermolecular interaction , as well as in quantitative analysis.
T-L-2The interpretation of HNMR spectra as a key to the determination of the structure of organic compounds.
T-L-3The application of IR method in qualitative and quantitative analysis of organic compounds.
T-L-4The application of chromatographic method in qualitative and quantitative analysis of multicomponent mixtures.
T-L-5The determination of some metals with the use of ASA method.
Metody nauczaniaM-2Classes
M-3Laboratory
Sposób ocenyS-2Ocena formująca: Assessment of laboratory written report.
S-3Ocena formująca: Assessment of homework assignments.
S-4Ocena formująca: Evaluation of the student’s work based on the student activity during the course.
Kryteria ocenyOcenaKryterium oceny
2,0
3,0Student is able to carry out the experiment with the simple interpretation of obtained results.
3,5
4,0
4,5
5,0
PoleKODZnaczenie kodu
Zamierzone efekty kształceniaWM-WTiICh_2-_null_K01Student is able to choose the appropriate method in order to solve particular problem concerning qualitative and/or quantitative analysis
Cel przedmiotuC-1Theoretical and practical learning about instrumental methods applied in quantitative and qualitative analysis;
Treści programoweT-L-1Measurements of UV-vis spectra and their application in the studies of solute-solvent intermolecular interaction , as well as in quantitative analysis.
T-L-2The interpretation of HNMR spectra as a key to the determination of the structure of organic compounds.
T-L-3The application of IR method in qualitative and quantitative analysis of organic compounds.
T-L-4The application of chromatographic method in qualitative and quantitative analysis of multicomponent mixtures.
T-L-5The determination of some metals with the use of ASA method.
T-W-4Theoretical studies of phenomena proceeding in the molecule/atom under the irradiation and their application in particular methods i.e. ultraviolet-visual spectroscopy (UV-VIS), infrared spectroscopy (IR), nuclear magnetic resonance spectroscopy (NMR), mass spectroscopy (MS), atomic absorption spectroscopy (AAS), X-ray absorption, atomic emission spectroscopy (AES), flame photometry, inductively coupled plasma spectrometry (ICP), X-ray fluorescence (XRF), atomic fluorescence.
T-W-5Explanation of phenomena, concepts, and definitions used in chromatographic methods. The ways of separation of a mixture components.
Metody nauczaniaM-1The lectures with the discussion.
M-3Laboratory
Sposób ocenyS-4Ocena formująca: Evaluation of the student’s work based on the student activity during the course.
Kryteria ocenyOcenaKryterium oceny
2,0
3,0Student is able to choose the appropriate method in order to solve the problem concerning quantitative analysis.
3,5
4,0
4,5
5,0